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Experimental Study of Silica Nano-Powder Synthesis Using a Diffusion Flame Reactor
1Indian Institute of Technology Kanpur, email@example.com
2Indian Institute of Technology Kanpur, firstname.lastname@example.org
3Indian Institute of Technology Kanpur, email@example.com
Citation Information: International Journal of Chemical Reactor Engineering. Volume 8, Issue 1, Pages –, ISSN (Online) 1542-6580, DOI: 10.2202/1542-6580.2246, October 2010
- Published Online:
A chemical reactor is designed and developed to synthesize silica nano-powders by oxidation of tetraethyl orthosilicate (TEOS) using a three-port diffusion flame burner. Nano-silica powders were successfully synthesized. The particle size of the silica powders were confirmed by AFM and TEM techniques. Scanning electron microscopy (SEM) reveals that as-synthesized silica powders are in agglomerated condition. Phase analysis using XRD shows that the nano-silica in as-prepared condition is in amorphous form. However, during subsequent heat-treatment, it becomes crystalline.