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Zeitschrift für Kristallographie - Crystalline Materials

Editor-in-Chief: Pöttgen, Rainer

Ed. by Antipov, Evgeny / Bismayer, Ulrich / Boldyreva, Elena V. / Huppertz, Hubert / Petrícek, Václav / Tiekink, E. R. T.


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The molecular and crystal structure of d,l-4-methoxy-6-styryl-5,6-dihydro-α-pyrone (kavain)*

Akie Yoshino / W. Nowacki

Citation Information: Zeitschrift für Kristallographie. Volume 136, Issue 1-2, Pages 66–80, ISSN (Online) 0044-2968, ISSN (Print) 1433-7266, DOI: 10.1524/zkri.1972.136.1-2.66, July 2010

Publication History

Published Online:
2010-07-28

Abstract

The crystal structure of kavain, C14H14O3, has been determined by x-ray diffraction methods. The crystals are monoclinic with space group P21/a. The unit-cell dimensions are a = 23.032 Å, b = 9.430 Å, c = 5.738 Å and β = 104°14′. There are four molecules in the unit cell. The structure was solved by the symbolic-addition method. The refinement was carried out by the block-matrix least-squares calculations including anisotropic temperature factors. The final R value for 1384 observed reflections was 0.076.

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[2]
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