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Zeitschrift für Kristallographie - Crystalline Materials

Ed. by Antipov, Evgeny / Bismayer, Ulrich / Huppertz, Hubert / Petrícek, Václav / Pöttgen, Rainer / Schmahl, Wolfgang / Tiekink, E. R. T. / Zou, Xiaodong

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Crystal and molecular structure of hexa(antipyrine)cadmium(II) perchlorate, [(C11H12ON2)6Cd]2+ [ClO4]2

C. Mahadevan / Akella Radha / M. Seshasayee

Citation Information: Zeitschrift für Kristallographie. Volume 169, Issue 1-4, Pages 159–163, ISSN (Online) 0044-2968, ISSN (Print) 1433-7266, DOI: 10.1524/zkri.1984.169.1-4.159, August 2010

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The crystal and molecular structure of the title compound is reported. Crystals are trigonal with hexagonal axes, space group P[unk] with Z = 1 in a unit cell of dimensions a = b = 14.196(7) and c = 9.558(5) Å. The structure was solved by the heavy-atom method and refined by the full-matix least-squares method to R = 0.071 for 1097 unique reflections. The metal atom of the cation has a regular octahedral configuration and the chlorine atoms of the anions have regular tetrahedral configuration. Both the five- and six-membered rings in the antipyrine are planar having an angle of 113° between the normals to their planes.

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