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Zeitschrift für Kristallographie - Crystalline Materials

Ed. by Antipov, Evgeny / Bismayer, Ulrich / Huppertz, Hubert / Petrícek, Václav / Pöttgen, Rainer / Schmahl, Wolfgang / Tiekink, E. R. T. / Zou, Xiaodong

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Collecting 3D electron diffraction data by the rotation method

Daliang Zhang1 / Peter Oleynikov2 / Sven Hovmöller* / Xiaodong Zou3

1 Stockholm University, Dep. of Materials and Environmental Chemistry, Stockholm, Schweden

2 Stockholm University, Dep. of Materials and Environmental Chemistry, Stockholm, Schweden

3 Stockholm University, Dep. of Materials and Environmental Chemistry, Stockholm, Schweden

* Correspondence address: Stockhom University, Dep. of Materials and Environmental Chemistry, Inorganic and Structural Chemistry, SE - 106 9 Stockholm, Schweden,

Citation Information: Zeitschrift für Kristallographie International journal for structural, physical, and chemical aspects of crystalline materials. Volume 225, Issue 2-3, Pages 94–102, ISSN (Print) 0044-2968, DOI: 10.1524/zkri.2010.1202, April 2010

Publication History

Published Online:
2010-04-16

This article offers supplementary material which is provided at the end of the article.

Abstract

A new method for collecting complete three-dimensional electron diffraction data is described. Diffraction data is collected by combining electron beam tilt at many very small steps, with rotation of the crystal in a few but large steps. A number of practical considerations are discussed, as well as advantages and disadvantages compared to other methods of collecting electron diffraction data.

Keywords: Electron diffraction; Data collection; 3D diffraction data

Supplementary Article Materials

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