Skip to content
Licensed Unlicensed Requires Authentication Published by De Gruyter May 12, 2021

Characterization and thermal properties of chitosan/perlite nanocomposites

  • Mehmet Doğan EMAIL logo , Hatice Yüksel and Berna Koçer Kizilduman

Abstract

In this study, chitosan/perlite nanocomposites were synthesized using the solvent casting method and then characterized using Fourier transform infrared spectroscopy, X-ray diffraction, optical contact angle, differential thermal analysis/thermogravimetry, differential scanning calorimetry, atomic force microscopy, transmission electron microscopy and Zetasizer NanoS devices. Perlite was determined to be dispersed in nano size and homogeneously in the chitosan matrix. Chitosan/perlite nanocomposite was generally more thermally stable compared to pure chitosan polymer. The fact that the amount of perlite in the nanocomposite increased showed that the hydrophilic properties of nanocomposites increased. In addition, antibacterial activities of the samples were investigated using the agar-disk diffusion method and hemocompatibility testing was also performed.


Prof.Dr. Mehmet Doğan Faculty of Science and Literature, Department of Chemistry Balikesir University Çağış-Balikesir 10145 TURKEY Tel.: +90 266 612 10 00/134105 Fax: +90 266 612 12 15

  1. Conflict of interest

    The authors declare that they have no conflict of interest.

References

[1] S.F. Wang, L. Shen, Y.J. Tong, L. Chen, I.Y. Phang, P.Q. Lim, T.X. Liu: Polym. Degrad. Stab. 90 (2005) 123. DOI:10.1016/j.polymdegradstab.2005.03.00110.1016/j.polymdegradstab.2005.03.001Search in Google Scholar

[2] M. Shahbazi, G. Rajabzadeh, S.J. Ahmadi: Carbohydr. Polym. 157 (2017) 226. DOI:10.1016/j.carbpol.2016.09.01810.1016/j.carbpol.2016.09.018Search in Google Scholar PubMed

[3] M.S.K. Sofla, S. Mortazavi, J. Seyfi: Carbohydr. Polym. 232 (2020) 115784. DOI:10.1016/j.carbpol.2019.11578410.1016/j.carbpol.2019.115784Search in Google Scholar PubMed

[4] D. Archana, B.K. Singha, J. Duttab, P.K. Dutta: Carbohydr. Polym. 95 (2013) 530. DOI:10.1016/j.carbpol.2013.03.03410.1016/j.carbpol.2013.03.034Search in Google Scholar PubMed

[5] M. Maruthupandy, G. Rajivgandhi, S. Kadaikunnan, T. Veeramani, N.S. Alharbi, T. Muneeswaran, J.M. Khaled, W. Jun-Li, K.F. Alanzi: Carbohydr. Polym. 230 (2020) 115646. DOI:10.1016/j.carbpol.2019.11564610.1016/j.carbpol.2019.115646Search in Google Scholar PubMed

[6] Y. Turhan, M. Doğan, M. Alkan: Ind. Eng. Chem. Res. 49 (2010) 1503. DOI:10.1021/ie901384x10.1021/ie901384xSearch in Google Scholar

[7] Y. Turhan, Z.G. Alp, M. Alkan, M. Doğan: Microporous Mesoporous Mater. 174 (2013) 144. DOI:10.1016/j.micromeso.2013.03.00210.1016/j.micromeso.2013.03.002Search in Google Scholar

[8] M. Doğan, M. Alkan, Ü. Çakır: J. Colloid Interface Sci. 192 (1997) 114. DOI:10.1006/jcis.1997.491310.1006/jcis.1997.4913Search in Google Scholar

[9] M. Doğan, M. Alkan, Y. Onganer: Water Air Soil Pollut. 120 (2000) 229. DOI:10.1023/A:100529772430410.1023/A:1005297724304Search in Google Scholar

[10] A. Sarı, A. Karaipekli, C. Alkan: Chem. Eng. J. 155 (2009) 899. DOI:10.1016/j.cej.2009.09.0010.1016/j.cej.2009.09.00Search in Google Scholar

[11] A. Karaipekli, A. Sarı, K. Kaygusuz: Energy Sources, Part A. 31 (2009) 814. DOI:10.1080/1556703070175276810.1080/15567030701752768Search in Google Scholar

[12] N. Arsalani, M. Hayatifar: J. Appl. Polym. Sci. 93 (2004) 2528. DOI:10.1002/app.2072010.1002/app.20720Search in Google Scholar

[13] S. Kalyani, J. Ajitha Priya, P. Srinivasa Rao, A. Krishnaiah: Sep. Sci. Technol. 40 (2005) 1483. DOI:10.1081/SS-20005594010.1081/SS-200055940Search in Google Scholar

[14] J.W. Rhim, S.I. Hong, H.M. Park, K.W. Ng. Perry: J. Agric. Food Chem. 54 16 (2006) 5814. DOI:10.1021/jf060658 h10.1021/jf060658hSearch in Google Scholar PubMed

[15] R. Jayakumar, D. Menon, K. Manzoor, S.V. Nair, H. Tamur: Carbohydr. Polym. 82 (2010) 227. DOI:10.1016/j.carbpol.2010.04.07410.1016/j.carbpol.2010.04.074Search in Google Scholar

[16] P. Demirçivi: Int. J. Biol. Macromol. 118 (2018) 340. DOI:10.1016/j.ijbiomac.2018.06.06510.1016/j.ijbiomac.2018.06.065Search in Google Scholar PubMed

[17] B.K. Kızılduman, M. Alkan, M. Doğan, Y. Turhan: Adv. Mater. Sci. 17 3 (2017) 5. DOI:10.1515/adms-2017-001210.1515/adms-2017-0012Search in Google Scholar

[18] V. Thomas, M.M. Yallapu, B. Sreedhar, S.K. Bajpai: J. Colloid Interface Sci. 315 1 (2007) 389. DOI:10.1016/j.jcis.2007.06.06810.1016/j.jcis.2007.06.068Search in Google Scholar PubMed

[19] D.Motlagh, J. Allen, R. Hoshi, J. Yang, K. Lui, G. Ameer: J. Biomed. Mater. Res. A, 82 (2007) 907. DOI:10.1002/jbm.a.3121110.1002/jbm.a.31211Search in Google Scholar PubMed

[20] R.M. Silverstein, F.X. Webster: Sixth ed. John Wiley Pub. Wiley India Pvt. Ltd. (2006) 88.Search in Google Scholar

[21] C. Khatri, A. Rani: Fuel. 87 (2008) 2886. DOI:10.1016/j.fuel.2008.04.01110.1016/j.fuel.2008.04.011Search in Google Scholar

[22] A. Karaipekli, A. Biçer, A. Sarı, V.V. Tyagi: Energy Convers. Manag. 134 15 (2017) 373. DOI:10.1016/j.enconman.2016.12.05310.1016/j.enconman.2016.12.053Search in Google Scholar

[23] S. Kabra, A. Sharma, S. Katara, R. Hada, A. Rani: Indian J. Appl. Res. 3 4 (2013) 40.Search in Google Scholar

[24] S.H. Javed, S. Naveed, N. Feroze, M. Zafar, M. Shafaq: J. of Quality and Technology Management. 6 1 (2010) 81.Search in Google Scholar

[25] D. Kadam, B. Momin, S. Palamthodi, S.S. Lele: Carbohydr: Polym. 211 (2019) 124. DOI:10.1016/j.carbpol.2019.02.00510.1016/j.carbpol.2019.02.005Search in Google Scholar

[26] D.D.L. Chung: Science and Applications 2nd Ed. P.B. Derby London: Springer-Verlag. (2010).Search in Google Scholar

[27] J.W. Rhim: Carbohydr: Polym. 86 2 (2011) 691. DOI:10.1016/j.carbpol.2011.05.01010.1016/j.carbpol.2011.05.010Search in Google Scholar

[28] H. Nolte, C. Schilde, A. Kwade: Compos. Sci. Technol. 72 9 (2012) 948. DOI:10.1016/j.compscitech.2012.03.01010.1016/j.compscitech.2012.03.010Search in Google Scholar

[29] P.Z. Hong, S.D. Li, C.Y. Ou, C.P. Li, L. Yang, C.H. Zhang: J. Appl. Polym. Sci. 105 (2007) 547. DOI:10.1002/app.2592010.1002/app.25920Search in Google Scholar

[30] J. Ratto, T. Hatakeyama, R.B. Blumstein: Polymer. 36 15 (1995) 2915. DOI:10.1016/0032-3861(95)94340-Y10.1016/0032-3861(95)94340-YSearch in Google Scholar

[31] K. Sakurai, T. Maegawa, T. Takahashi: Polymer.41 19 (2000) 7051. DOI:10.1016/S0032-3861(00)00067-710.1016/S0032-3861(00)00067-7Search in Google Scholar

[32] F. Kittur, K.H. Prashanth, K.U. Sankar, R. Tharanathan: Carbohydr: Polym. 49 2 (2002) 185. DOI:10.1016/S0144-8617(01)00320-410.1016/S0144-8617(01)00320-4Search in Google Scholar

[33] U. Ajdnik, M. Finsgar, L.F. Zemljic: Carbohydr: Polym. 232 (2020) 115817. DOI:10.1016/j.carbpol.2019.11581710.1016/j.carbpol.2019.115817Search in Google Scholar PubMed

[34] G.M. Shanthini, C. Ann, N. Sakthivel, S. Chandra, K. Elayaraja, B.S. Lakshmi, K. Asokan, D. Kanjilal, S.N. Kalkura: Appl. Surf. Sci. 329 (2015) 116. DOI:10.1016/j.apsusc.2014.12.12910.1016/j.apsusc.2014.12.129Search in Google Scholar

[35] M.A. Rahman, B. Ochiai: Microsyst. Technol. 24 (2018) 669. DOI:10.1007/s00542-017-3318-810.1007/s00542-017-3318-8Search in Google Scholar

[36] J.P. Singhal, A.R. Ray: Biometarials. 23 4 (2002) 1139. DOI:10.1016/s0142-9612(01)00228-910.1016/s0142-9612(01)00228-9Search in Google Scholar

Received: 2020-07-29
Accepted: 2021-02-10
Published Online: 2021-05-12
Published in Print: 2021-05-31

© 2021 Walter de Gruyter GmbH, Berlin/Boston, Germany

Downloaded on 19.3.2024 from https://www.degruyter.com/document/doi/10.1515/ijmr-2020-8007/html
Scroll to top button