Synthesis, structure, and magnetic properties of the quaternary oxysulfides Ln
5V3O7S6 (Ln = La, Ce)

Chong Zheng; Roald Hoffmann; Timothy S. Perkins; Frank Calvagna; Roxanna Fotovat; Crystal Ferels; Alyssa Mohr; Reinhard K. Kremer; Jürgen Köhler; Arndt Simon; Kejun Bu; Fuqiang Huang

doi:10.1515/znb-2021-0107

Published by De Gruyter September 22, 2021

Synthesis, structure, and magnetic properties of the quaternary oxysulfides Ln ₅V₃O₇S₆ (Ln = La, Ce)

Chong Zheng , Roald Hoffmann , Timothy S. Perkins , Frank Calvagna , Roxanna Fotovat , Crystal Ferels , Alyssa Mohr , Reinhard K. Kremer , Jürgen Köhler , Arndt Simon , Kejun Bu and Fuqiang Huang

From the journal Zeitschrift für Naturforschung B

https://doi.org/10.1515/znb-2021-0107

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Abstract

Two rare earth oxysulfides Ln ₅V₃O₇S₆ (Ln = La, Ce) have been synthesized and their structures determined. The two isostructural compounds crystallize in the orthorhombic space group Pmmn (no. 59). The structure features one-dimensional edge-sharing VS₄O₂ octahedron chains parallel to the b axis. The bonding between V and S/O is covalent, and between Ln ³⁺ and the rest of the matrix ionic. Magnetic susceptibility measurement revealed that V is in a mixed valence state of V³⁺ and V⁴⁺. Its magnetic behavior follows the Curie-Weiss law.

Keywords: cerium; lanthanum; oxysulfide; quaternary compound; vanadium

Dedicated to: Professor Richard Dronskowski of the RWTH Aachen on the occasion of his 60th birthday.

Corresponding authors: Chong Zheng and Roald Hoffmann, Department of Chemistry and Biochemistry, Northern Illinois University, DeKalb, IL, 60115, USA; and Department of Chemistry and Chemical Biology, Cornell University, Ithaca, New York 14853, USA, E-mail: czheng@niu.edu (C. Zheng), rh34@cornell.edu (R. Hoffmann)

Author contributions: All the authors have accepted responsibility for the entire content of this submitted manuscript and approved submission.
Research funding: None declared.
Conflict of interest statement: The authors declare no conflicts of interest regarding this article.

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Supplementary Material

The online version of this article offers supplementary material (https://doi.org/10.1515/znb-2021-0107).

Received: 2021-08-04

Accepted: 2021-08-22

Published Online: 2021-09-22

Published in Print: 2021-11-25

Synthesis, structure, and magnetic properties of the quaternary oxysulfides Ln ₅V₃O₇S₆ (Ln = La, Ce)

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Synthesis, structure, and magnetic properties of the quaternary oxysulfides Ln ₅V₃O₇S₆ (Ln = La, Ce)