You currently have no access to view or download this content. Please log in with your institutional or personal account if you should have access to this content through either of these.
Showing a limited preview of this publication:
Abstract
Lead acetate trihydrate crystallizes in a tetramolecular, monoclinic unit cell of dimensions a = 15.85(1), b = 7.30(1), c = 9.10(1) Å, β = 109.8(5)° in the space group C2/m. The crystal structure has been solved by the heavy-atom method and refined to an R value of 0.096 for 790 observed reflections. Nine oxygen atoms belonging to the water molecules and acetate groups coordinate the lead atom whose coordination polyhedron is a monocapped square antiprism. The two crystallographically different acetate groups coordinate both bidentally to the same metal atom. A hydrogen bonding scheme based on the distance criteria has been proposed.
Published Online: 2010-08-25
Published in Print: 1982