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BY-NC-ND 3.0 license Open Access Published by De Gruyter Open Access October 6, 2009

High surface area nano-sized La0.6Ca0.4MnO3 perovskite powder prepared by low temperature pyrolysis of a modified citrate gel

Meysam Soleymani EMAIL logo , Ahmad Moheb and Ezatolah Joudaki
From the journal Open Chemistry

Abstract

Single phase nanocrystalline La0.6Ca0.4MnO3 powder was synthesized by both the usual and a modified citrate gel precursor method, and the effects on the formation of homogeneous nano-sized powder with a perovskite structure were investigated. In the modified method, single phase La0.6Ca0.4MnO3 powder with an average particle size of 17.2 nm was obtained when the powder was pyrolyzed at 520°C for 2 h. Its specific surface area was 40.7 m2 g−1, about 4-fold larger than that of powder made by the usual citrate gel method.

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Published Online: 2009-10-6
Published in Print: 2009-12-1

© 2009 Versita Warsaw

This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License.

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