Skip to content
Licensed Unlicensed Requires Authentication Published by De Gruyter April 22, 2016

Effect of indentation conditions on the cracking behavior of a FeCrBSi coating

Auswirkungen der Eindruckbedingungen auf das Rissverhalten einer FeCrBSi-Beschichtung
  • Ya-nan Song , Bin-shi Xu , Hai-dou Wang , Ming Liu and Zhong-yu Piao
From the journal Materials Testing

Abstract

A detector combining indentation method and acoustic emission (AE) technique was developed for evaluating the bonding strengths of sprayed coatings. In order to study the effect of indentation conditions on cracking failure behavior of sprayed coating, FeCrBSi coating was prepared by plasma spraying technique. The AE signals during indentation test were abstracted and investigated. The morphologies of indented samples were observed by scanning electronic microscopy (SEM). The results indicate that indentation equipment can induce the cracking failure of coating and AE technique can define the critical statues. The test by interior load was feasible and accurate for evaluating the bonding strength. The key influential factor of indenter lied in the contact area between indenter and coating. The loading rate had little effect on AE signal. The loading conditions were optimized to use diamond indenter with interior load and a loading rate of 100 pulses per second.

Kurzfassung

In der diesem Beitrag zugrunde liegenden Studie wurde ein Detektor entwickelt, der das Eindruckverfahren mit der akustischen Emmissiontechnik (Acoustic Emission (AE)) kombiniert, um die Bindungsfestigkeit von Spritzschichten zu bestimmen. Um die Auswirkungen der Eindruckbedingungen auf das Rissverhalten von Spritzschichten zu untersuchen, wurde eine FeCrBSi-Beschichtung mittels Plasmaspritzens vorbereitet. Die akustischen Emissionssignale während des Eindringversuches wurden abstrahiert und untersucht. Die Morphologien der eingedrückten Proben wurden mittels Rasterelektronenmikroskopie (REM) untersucht. Die Ergebnisse deuten darauf hin, dass mit der Eindruck-Vorrichtung Risse in der Beschichtung verursacht werden können und dass die AE-Technik den kritischen Zustand diesbezüglich bestimmen kann. Der Versuch mit interner Belastung war durchführbar und genau, um die Bindungsfestigkeit zu berechnen. Der Haupteinflußfaktor auf den Eindringkörper war die Berührungsfläche zwischen Eindringkörper und Beschichtung. Die Belastungsgeschwindigkeit hatte dabei einen geringen Effekt auf das AE-Signal. Die Belastungsbedingungen wurden optimiert, um einen Diamant-Indenter bei interner Belastung und einer Belastungsgeschwindigkeit von 100 Pulsen pro Sekunde zu verwenden.


*Correspondence Address, Dr. Hai-dou Wang, National Key Laboratory for Remanufacturing, Academy of Armored Forces Engineering, No.21 Dujiakan, Fengtai District, Beijing, 100072, PR China, E-mail:

Ya-nan Song, born in 1987, graduated with a Master of Science in Materials Science and Engineering from the Academy of Armored Forces Engineering, Beijing, China, in 2012. He continued studying for a Doctor's degree at the same faculty in March 2013. His main research areas include spraying process optimization and performance evaluation of surface coatings.

Prof. Bin-shi Xu, member of the Chinese Academy of Engineering, born in 1931, graduated with a Bachelor's degree from Harbin Institute of Technology in Mechanism Manufacturing and Welding, in 1954. He works as Professor at the National Key Laboratory for Remanufacturing, Academy of Armored Forces Engineering, Beijing, China. He is a leading expert in equipment maintenance engineering, surface engineering and remanufacturing engineering.

Dr. Hai-dou Wang, born in 1969, received his PhD from the Department of Mechanical Engineering, Tsinghua University, Beijing, China, in 2003. He works as Professor at the National Key Laboratory for Remanufacturing, Academy of Armored Forces Engineering, Beijing, China. He has studied at George Washington University as a visiting scholar for one year. His main research interests include remanufacturing engineering, surface engineering and basic theory in tribology.

Ming Liu, born in 1979, graduated with a Master of Science in Materials Science and Engineering from the Academy of Armored Forces Engineering, Beijing, China, in 2006. Now, he works as a lecturer and is studying for a Doctor's degree at the same faculty. His main researches focus on surface coatings and plasma spraying techniques.

Dr. Zhong-yu Piao, born in 1982, graduated with a Doctor's degree in Machinery Design and Theory from Yanshan University, China in 2011. He works as Associate Professor at the College of Mechanical Engineering, Zhejiang University of Technology, Hangzhou, China. His main research interests focus on life prediction for manufacturing products.


References

1 H. D.Wang, B. S.Xu, J. J.Liu, D. M.Zhuang: Characterization and tribological properties of plasma sprayed FeS solid lubrication coatings, Materials Characterization55 (2005), No. 1, pp. 434910.1016/j.matchar.2005.02.007Search in Google Scholar

2 I. D.Uţu, I.Mitelea: SNMS investigations of thermally sprayed coatings, Materials Testing57 (2015), No. 3, pp. 26727210.3139/120.110706Search in Google Scholar

3 S.Özel, H.Turhan: Plasma spray coating of an AA 2024-T4 Al alloy with oxide powders, Materials Testing52 (2010), No. 4, pp. 25225610.3139/120.110126Search in Google Scholar

4 Y. L.Wang, Z. H.Jiang, Z. P.Yao: Microstructure, bonding strength and thermal shock resistance of ceramic coatings on steels prepared by plasma electrolytic oxidation, Applied Surface Science256 (2009), No. 3, pp. 65065610.1016/j.apsusc.2009.08.036Search in Google Scholar

5 A.Vencl, S.Arostegui, G.Favaro, F.Zivic, M.Mrdak, S.Mitrovic, V.Popovic: Evaluation of adhesion/cohesion bond strength of the thick plasma spray coatings by scratch testing on coatings cross-sections, Tribology International44 (2011), No. 11, pp. 1281128810.1016/j.triboint.2011.04.002Search in Google Scholar

6 K.Cheng, C. B.Ren, W. J.Weng, P. Y.Du, G.Shen, G. R.Han, S.Zhang: Bonding strength of fluoridated hydroxyapatite coatings: A comparative study on pull-out and scratch analysis, Thin Solid Films517 (2009), No. 17, pp. 5361536410.1016/j.tsf.2009.03.122Search in Google Scholar

7 Y.Peng, C.Zhang, H.Zhou, L.Liu: On the bonding strength in thermally sprayed Fe-based amorphous coatings, Surface and Coatings Technology218 (2013), pp. 172210.1016/j.surfcoat.2012.12.018Search in Google Scholar

8 V. Y.Mehr, M. R.Toroghinejad, A.Rezaeian: The effect of oxide film and annealing treatment on the bond strength of Al-Cu strips in cold roll bonding process, Materials & Design53 (2014), pp. 17418110.1016/j.matdes.2013.06.028Search in Google Scholar

9 H.Zhang, D. Y.Li: Application of a novel lateral force-sensing microindentation method for evaluation of the bond strength of thermal sprayed coatings, Surface and Coatings Technology197 (2005), No. 2–3, pp. 13714110.1016/j.surfcoat.2004.06.038Search in Google Scholar

10 R.Rabe, J.-M.Breguet, P.Schwaller, S.Stauss, F.-J.Haug, J.Patscheider, J.Michler: Observation of fracture and plastic deformation during indentation and scratching inside the scanning electron microscope, Thin Solid Films469–470 (2004), pp. 20621310.1016/j.tsf.2004.08.096Search in Google Scholar

11 J.von Stebut, F.Lapostolle, M.Bucsa, H.Vallen: Acoustic emission monitoring of single cracking events and associated damage mechanism analysis in indentation and scratch testing, Surface and Coatings Technology116–119 (1999), pp. 16017110.1016/S0257-8972(99)00211-XSearch in Google Scholar

12 C. K.Tan, P.Irving, D.Mba: A comparative experimental study on the diagnostic and prognostic capabilities of acoustics emission, vibration and spectrometric oil analysis for spur gear, Mechanical Systems and Signal Processing21 (2007), No. 1, pp. 20823310.1016/j.ymssp.2005.09.015Search in Google Scholar

13 C.Wang, T.Bao, H.Lu, L.Liu, Z.Lu, W.Li, Q.Yu: Variation regulation of the acoustic emission energy parameter during the failure process of granite under uniaxial compression, Materials Testing57 (2015), No. 9, pp. 75576010.3139/120.110776Search in Google Scholar

14 P. L.Larsson, I. R. M.Peterson: Evaluation of sharp indentation testing of thin films and ribbons on hard substrates, Journal of Testing and Evaluation30 (2002), No. 1, pp. 647310.1520/JTE12290JSearch in Google Scholar

15 L.Prchlik, J.Pisacka, S.Sampath: Deformation and strain distribution in plasma sprayed nickel-aluminum coating loaded by a spherical indenter, Materials Science and Engineering A360 (2003), No. 1–2, pp. 26427410.1016/S0921-5093(03)00414-3Search in Google Scholar

16 D. W.Schwach, Y. B.Guo: A fundamental study on the impact of surface integrity by hard turning on rolling contact fatigue, International Journal of Fatigue28 (2006), No. 12, pp. 1838184410.1016/j.ijfatigue.2005.12.002Search in Google Scholar

17 W. Q.Qiu, Z. W.Liu, L. X.He, D. C.Zeng, Y.-W.Mai: Improved interfacial adhesion between diamond film and copper substrate using a Cu(Cr)-diamond composite interlayer, Materials Letters81 (2012), pp. 15515710.1016/j.matlet.2012.05.015Search in Google Scholar

18 W. Q.Qiu, A.Dasari, Y.-W.Mai: Improvement in adhesion of diamond film on Cu substrate with an inlay structured interlayer, Surface and Coatings Technology206 (2011), No. 2–3, pp. 22422710.1016/j.surfcoat.2011.06.048Search in Google Scholar

19 N. H.Faisal, R.Ahmed, Y. Q.Fu, Y. O.Elakwah, M.Alhoshan: Influence of indenter shape on DLC film failure during multiple load cycle nanoindentation, Materials Science and Technology28 (2012), No. 9–10, pp. 1186119710.1179/1743284712Y.0000000039Search in Google Scholar

20 H. T.Wang, S. Q.Zhang, J. H.Huang, J. L.Zhu, H.Zhang, X. K.Zhao: Fabrication of TiC-Fe cermet coating by plasma spraying of Fe-Ti-C powder using sucrose as carbon source, Materials Science and Technology26 (2010), No. 5, pp. 57958510.1179/174328409X448466Search in Google Scholar

21 R.Ahmed, N. H.Faisal, N. M.Al-Anazi, S.Al-Mutairi, F.-L.Toma, L.-M.Berger, A.Potthoff, E. K.Polychroniadis, M.Sall, D.Chaliampalias, M. F. A.Goosen: Structure property relationship of suspension thermally sprayed WC-Co nanocomposite coatings, Journal of Thermal Spray Technology24 (2015), No. 3, pp. 35737710.1007/s11666-014-0174-2Search in Google Scholar

22 N. H.Faisal, R.Ahmed, A. K.Prathuru, S.Spence, M.Hossain, J. A.Steel: An improved Vickers indentation fracture toughness model to assess the quality of thermally sprayed coatings, Engineering Fracture Mechanics128 (2014), pp. 18920410.1016/j.engfracmech.2014.07.015Search in Google Scholar

23 Z. Y.Piao, B. S.Xu, H. D.Wang, D. H.Wen: Investigation of RCF failure prewarning of Fe-based coating by online monitoring, Tribology International72 (2014), pp. 15616010.1016/j.triboint.2013.12.016Search in Google Scholar

24 Z. Y.Piao, B. S.Xu, H. D.Wang, D. H.Wen: Investigation of acoustic emission source of Fe-based sprayed coating under rolling contact, International Journal of Fatigue47 (2013), pp. 18418810.1016/j.ijfatigue.2012.08.011Search in Google Scholar

25 Z.Song, X.Bao, U.Wild, M.Muhler, G.Ertl: Oxidation of amorphous Ni-Zr alloys studied by XPS, UPS, ISS and XRD, Applied Surface Science134 (1998), No. 1–4, pp. 313810.1016/S0169-4332(98)00249-9Search in Google Scholar

26 J.Tao, X. Z.Guo, Z. D.Huang, H. B.Liu, T.Wang: Preparation and characterization of enamel coating on pure titanium as a hydrogen penetration barrier, Nuclear Engineering and Design259 (2013), pp. 657010.1016/j.nucengdes.2013.02.041Search in Google Scholar

27 N. H.Faisal, R.Ahmed, R. L.Reuben: Indentation testing and its acoustic emission response: Applications and emerging trends, International Materials Reviews56 (2011), No. 2, pp. 9814210.1179/1743280410Y.0000000004Search in Google Scholar

28 M.Ahadi, M. S.Bakhtiar: Leak detection in water-filled plastic pipes through the application of tuned wavelet transforms to acoustic emission signals, Applied Acoustics71 (2010), No. 7, pp. 63463910.1016/j.apacoust.2010.02.006Search in Google Scholar

29 H.Roy, N.Parida, S.Sivaprasad, S.Tarafder, K. K.Ray: Acoustic emission during fracture roughness tests of steels exhibiting varying ductility, Materials Science and Engineering A486 (2008), No. 1–2, pp. 56257110.1016/j.msea.2007.09.036Search in Google Scholar

30 K. R.Al-Balushi, A.Addali, B.Charnley, D.Mba: Energy index technique for detection of acoustic emissions associated with incipient bearing failures, Applied Acoustics71 (2010), No. 9, pp. 81282110.1016/j.apacoust.2010.04.006Search in Google Scholar

31 C. E.Everson, S. H.Cheraghi: The application of acoustic emission for precision drilling process monitoring, International Journal of Machine Tools and Manufacture39 (1999), No. 3, pp. 3713810.1016/S0890-6955(98)00054-6Search in Google Scholar

32 S.Al-Dossary, R. I. R.Hamzah, D.Mba: Observations of changes in acoustic emission waveform for varying seeded defect sizes in a rolling element bearing, Applied Acoustics70 (2009), No. 1, pp. 588110.1016/j.apacoust.2008.01.005Search in Google Scholar

33 R.Danzer: On the relationship between ceramic strength and the requirements for mechanical design, Journal of the European Ceramic Society34 (2014), No. 15, pp. 3435346010.1016/j.jeurceramsoc.2014.04.026Search in Google Scholar

34 P. L.Larsson: On the mechanical behavior of global parameters in material characterization by sharp indentation testing, Journal of Testing and Evaluation32 (2004), No. 4, pp. 31032110.1520/JTE11851Search in Google Scholar

35 Z. Y.Piao, B. S.Xu, H. D.Wang, C. H.Pu: Investigation of fatigue failure prediction of Fe-Cr alloy coatings under rolling contact based on acoustic emission technique, Applied Surface Science257 (2011), No. 7, pp. 2581258610.1016/j.apsusc.2010.10.026Search in Google Scholar

36 J.Li, T. W.Chou: Elastic field of a thin-film/substrate system under an axisymmetric loading, International Journal of Solids and Structures34 (1997), No. 35–36, pp. 4463447810.1016/S0020-7683(97)00053-XSearch in Google Scholar

37 H.Chai: Fracture mechanics analysis of thin coatings under plane-strain indentation, International Journal of Solids and Structures40 (2003), No. 3, pp. 59161010.1016/S0020-7683(02)00619-4Search in Google Scholar

38 H.Chai: Transverse fracture in thin-film coatings under spherical indentation, Acta Materialia53 (2005), No. 2, pp. 48749810.1016/j.actamat.2004.10.006Search in Google Scholar

39 S.Wuttiphan, A.Pajares, B. R.Lawn, C. C.Berndt: Effect of substrate and bond coat on contact damage in zirconia-based plasma-sprayed coatings, Thin Solid Films293 (1997), No. 1–2, pp. 25126010.1016/S0040-6090(96)08992-4Search in Google Scholar

40 G. B.Neighbour, B.Mcenaney: An investigation of acoustic emission from an irradiated nuclear graphite, Journal of Nuclear Materials223 (1995), No. 3, pp. 30531110.1016/0022-3115(95)00024-0Search in Google Scholar

41 C. K.Mukhopadhyay, T.Jayakumar, B.Raj, K. K.Ray: Acoustic emission-stress intensity factor relations for tensile deformation of notched specimens of AISI type 304 stainless steel, Materials Science and Engineering A293 (2000), No. 1–2, pp. 13714510.1016/S0921-5093(00)01042-XSearch in Google Scholar

Published Online: 2016-04-22
Published in Print: 2016-05-02

© 2016, Carl Hanser Verlag, München

Downloaded on 28.11.2023 from https://www.degruyter.com/document/doi/10.3139/120.110865/html
Scroll to top button