Skip to content
Licensed Unlicensed Requires Authentication Published by De Gruyter April 6, 2013

Rheological and Thermal Properties of a Model System for PIM

  • H. Persson , B. Hausnerová , L. Nyborg and M. Rigdahl

Abstract

Powder injection moulding (PIM) is an important and accepted industrial technique for net shaping of precision components which can have a rather complex geometry. In order to meet the imposed, often rather strict, requirements with regard to dimensional accuracy, it is important to have an adequate knowledge and control of the rheological behaviour and the related processing properties of the powder/polymer melt (feedstock). Such a knowledge is furthermore of crucial importance in numerical simulations of the PIM-process. In the present work, a model system, consisting of steel powder, poly(ethylene glycol) and wax, is used in order to illustrate how the viscometric properties as well as thermal properties, such as the conductivity and the specific heat, of the system can be related to the corresponding properties of the polymeric binder system. In a similar way, the pvT (pressure-volume-temperature)-behaviour of the model system is analysed and discussed. The pvT-behaviour, which has not been extensively reported on for PIM-feedstocks, is considered to be of significant relevance for controlling the outcome of the injection moulding process.


Mail address: Henrik Persson, Chalmers University of Technology, Department of Materials and Manufacturing Technology, SE-41296 Göteborg, Sweden. E-mail:

References

Araujo, F. F. T., Rosenberg, H. M., “The Thermal Conductivity of Epoxy-resin/Metal-powder Composite Materials from 1.7 to 300 K”, J. Phys. D: Appl. Phys., 9, 665675(1976)10.1088/0022-3727/9/4/017Search in Google Scholar

Barnes, H. A., Hutton, J. F., Walters, K.: An Introduction to Rheology, Elsevier, Amserdam(1989)Search in Google Scholar

Boyer, H. E., Gall, T. L.: Metal Handbook, Desk Edition, Amer. Soc. Metals, Ohio(1985)Search in Google Scholar

Dhami, A. K., et al., “Thermal Conductivity Of 2223 BSCCO Superconductor-Polyethylene Glycol Composites between 20 and 300 K”, J. Supercond., 13, 417422(2000)10.1023/A:1007755125840Search in Google Scholar

Fu, G., et al., “The demolding of Powder Injection Molded Micro-Structures: Analysis, Simulation And Experiments”, J. Micromech. Microeng., 18, 075024(2008). 10.1088/0960-1317/18/7/075024Search in Google Scholar

German, R. M., Bose, A.: Injection Moulding of Metals and Ceramics, Metal Powder Industries Federation, Princeton N. J.(1997)Search in Google Scholar

German, R. M.: Powder Injection Molding, Metal Powder Industries Federation, Princeton N. J.(1990)Search in Google Scholar

JMatPro version 4.0.5, Sente Software, Guildford, UK(2005)Search in Google Scholar

Johansson, E.: “Surface Interactions in Powder Injection Moulding”, PhD Thesis, Chalmers University of Technology, Göteborg, Sweden (2002)Search in Google Scholar

Johansson, E., Nyborg, L., “XPS Study of Surface-active Organic Compounds on Fine Ferrous Powder”, Surf. Interface Anal., 30, 333336(2000)10.1002/1096-9918(200008)30:1<333::AID-SIA843>3.0.CO;2-HSearch in Google Scholar

Johansson, E., et al., “Assessment of Rheology and Related Properties of OIM Feedstock Material”, Europ. Symp. Powder Injection Moulding, 67–74 (2000)Search in Google Scholar

Kowalski, L., Duszczyk, J., “Specific Heat of Metal powder-polymer Feedstock for Powder Injection Molding”, J. Mater. Sci. Letters, 18, 14171420(1999)10.1023/A:1006623507854Search in Google Scholar

Kowalski, L., et al., “Thermal Conductivity of Metal Powder-polymer Feedstock for Powder Injection Moulding”, J. Mater. Sci., 34, 15(1999)10.1023/A:1004424401427Search in Google Scholar

Meredith, R. E., Tobias, C. W., “Resistance to Potential Flow through Cubical Array of Spheres”, J. Appl. Phys., 31, 12701273(1960)10.1063/1.1735816Search in Google Scholar

Nyborg, L., et al., “Reaction Products on Metal Powder Surfaces and Interfaces”, Colloq. Controlling the Properties of PM Parts through their Microstructure, Paris (1990)Search in Google Scholar

Nyborg, L., et al., “Guide to Injection Moulding of Ceramics and Hardmetals: Special Consideration of Fine Powder”, Powder Metal, 41, 4145(1998)Search in Google Scholar

Parker, W. J., et al., “Flash Method of Determining Thermal Diffusivity, Heat Capacity and Thermal Conductivity”, J. Appl. Phys., 32, 16791684(1961)10.1063/1.1728417Search in Google Scholar

Van Krevelen, D. W.: Properties of Polymers, 3rd Edition, Elsevier, Amsterdam(1990)Search in Google Scholar

Zoller, P., Walsh, D. J.: Standard Pressure-Volume-Temperature Data for Polymers, Technomic Publishing, Lancaster(1995)Search in Google Scholar

Received: 2008-11-04
Accepted: 2009-02-11
Published Online: 2013-04-06
Published in Print: 2009-05-01

© 2009, Carl Hanser Verlag, Munich

Downloaded on 5.12.2023 from https://www.degruyter.com/document/doi/10.3139/217.2243/html
Scroll to top button