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, project No. 2/3100/23, and the Slovak–French Science and Technology Co-operation PROGRAMME STEFANIK are acknowledged for financial support. References 1. A. V. Vik, Structure and Solubility of Niobium and Tantalum Complexes in Molten Alkali Fluorides; Ph.D. Thesis, Norwegian University of Science and Technology, Trondheim (2000). 2. V. I. Konstantinov, Elektrovydelenie tantala, niobia a ich splavov (Electrodeposition of tantalun, niobium and their alloys). Metalurgia, Moskva (1977), p. 41. 3. V. Van, A. Silný, J. Hı́veš, and V. Daněk, Electrochem. Commun. 7 (1999