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Biophysical Chemistry, 37077 Göttingen, Germany IV Laboratory of Molecular Biophysics, Department of Biochemistry, University of Oxford, South Parks Road, Oxford, OX1 3QU, UK Received July 15, 2011; accepted November 2, 2011 Multigrain crystallography / 3DXRD microscopy / Crystal structure determination / Polycrystal diffraction / Crystal indexing Abstract. We summarize exploratory work on multi- grain crystallography. The experimental arrangement com- prises a monochromatic beam, a fully illuminated sample with up to several hundred grains in transmission geome- try on a