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  • "Tetrakis(trifluormethylthiolatooxo)rhenate(V)" x
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By ligand exchange reactions of (n-Bu4N )[ReOBr4] with NaI dissolved in acetone pure (n-Bu4N )[ReOI4], and with AgSCF3 suspended in dichloromethane (n-Bu4N )[ReO(SCF3)4] have been prepared for the first time. The vibrational spectra of both complexes are assigned according to point group C4v, supported by normal coordinate analysis based on a general valence force field. 13C and ,19F NMR spectra provide evidence for the equivalence o f the SCF3 groups.

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(difluorophosphona- to)palladate(II) C o m p le x ........................................ 737 Tetrakis(difluorophosphonato)palladate(II) Com­ plex Preparation and Reactions of Binuclear Plati- num(II) Complexes. Single Crystal X-Ray Dif­ fraction Study of a Tetrakis(difluorophosphona- to)palladate(II) C o m p le x ........................................ 737 Tetrakis(trifluormethylthiolatooxo)rhenate(V) Preparation and Spectroscopic Characterization Subject Index 1881 of the Oxorhenates(V), [ReOIJ and [ReO- (SCF3) J