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American Mineralogist

Journal of Earth and Planetary Materials

Ed. by Baker, Don / Xu, Hongwu / Swainson, Ian


IMPACT FACTOR 2017: 2.645

CiteScore 2017: 2.31

SCImago Journal Rank (SJR) 2017: 1.440
Source Normalized Impact per Paper (SNIP) 2017: 1.059

Online
ISSN
1945-3027
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Volume 93, Issue 5-6

Issues

Fracture toughness, hardness, and elastic modulus of kyanite investigated by a depth-sensing indentation technique

Alexandre Mikowski / Paulo Soares
  • Department of Mechanical Engineering, Pontifícia Universidade Católica do Paraná, Curitiba (PR) 80215-901, Brazil
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
/ Fernando Wypych / Carlos M. Lepienski
Published Online: 2015-04-01 | DOI: https://doi.org/10.2138/am.2008.2694

Abstract

Macroscopically bladed kyanite crystals of blue and glassy luster were cleaved along two planes, and the mechanical properties were measured through depth-sensing indentation (DSI). The conventional method to determine fracture toughness (KIC) from indentation is based on radial crack lengths measurements, which is difficult to estimate owing to the ease with which kyanite cleaves. An alternative method is proposed to determine the KIC for the perfect cleavage plane (100) of kyanite based on the estimation of the crack nucleation threshold load from a discontinuity or “pop-in” in the DSI load-unload curve. The toughness value for kyanite in the plane of perfect cleavage (100) determined by the proposed method is KIC =2.1 MPa·m1/2. The hardness of 10.7 ± 1.6 GPa for the perfect cleavage plane is lower than the one measured in a plane (010), 18.0 ± 2.9 GPa. The measured elastic modulus for the perfect cleavage plane (100) and for the plane (010) are 297 ± 11 and 405 ± 31 GPa, respectively. These values are in agreement with the published mechanical properties of kyanite, obtained by other techniques. The mechanical behavior is discussed and correlated to fracture patterns during indentation for both crystallographic directions of this mineral.

Keywords: Kyanite; fracture toughness; hardness; elastic modulus; depth-sensing indentation; mechanical properties

About the article

Received: 2007-05-14

Accepted: 2007-11-30

Published Online: 2015-04-01

Published in Print: 2008-05-01


Citation Information: American Mineralogist, Volume 93, Issue 5-6, Pages 844–852, ISSN (Online) 1945-3027, ISSN (Print) 0003-004X, DOI: https://doi.org/10.2138/am.2008.2694.

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