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Abstract
A method to determine the proportion of both enantiomers of 2,6-di-O-alkylgalactose in a permethylated/perethylated polysaccharide is described. It involves conversion of the monosaccharides, obtained by hydrolysis of the sample, to the corresponding diastereomeric acetylated 1-deoxy-1-(1-phenylethylamino)alditols, followed by gas chromatographic analysis. This procedure has been applied to a polysaccharide isolated from Pterocladiella capillacea.
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Published Online: 2005-06-01
Published in Print: 2001-02-27
Copyright © 2001 by Walter de Gruyter GmbH & Co. KG