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Clinical Chemistry and Laboratory Medicine (CCLM)

Published in Association with the European Federation of Clinical Chemistry and Laboratory Medicine (EFLM)

Editor-in-Chief: Plebani, Mario

Ed. by Gillery, Philippe / Greaves, Ronda / Lackner, Karl J. / Lippi, Giuseppe / Melichar, Bohuslav / Payne, Deborah A. / Schlattmann, Peter


IMPACT FACTOR 2018: 3.638

CiteScore 2018: 2.44

SCImago Journal Rank (SJR) 2018: 1.191
Source Normalized Impact per Paper (SNIP) 2018: 1.205

Online
ISSN
1437-4331
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Volume 41, Issue 12

Issues

Analysis of Nitrofuran Metabolites in Food by High-Performance Liquid Chromatography with Tandem Mass Spectrometry Detection

Patrick Edder / Sandra Vargas / Didier Ortelli / Claude Corvi
Published Online: 2005-06-01 | DOI: https://doi.org/10.1515/CCLM.2003.244

Abstract

A reliable and sensitive procedure is presented for the analysis of nitrofuran metabolite residues in foods of animal origin, like poultry and shrimp. The method is based on a one-step extraction/derivatization, followed by solid-phase extraction clean-up with polymeric phase cartridges. The separations were carried out by liquid chromatography coupled with tandem mass spectroscopy detection.

Results from the full validation of the procedure and from a survey of food available from the Swiss market, with the analysis of 236 samples of shrimp, poultry, fish and rabbit, are presented and demonstrate that this method is satisfactory in order to control nitrofuran residues in foods of animal origin.

About the article

Published Online: 2005-06-01

Published in Print: 2003-12-04


Citation Information: Clinical Chemistry and Laboratory Medicine, Volume 41, Issue 12, Pages 1608–1614, ISSN (Print) 1434-6621, DOI: https://doi.org/10.1515/CCLM.2003.244.

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