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Open Chemistry

formerly Central European Journal of Chemistry

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IMPACT FACTOR 2016 (Open Chemistry): 1.027
IMPACT FACTOR 2016 (Central European Journal of Chemistry): 1.460

CiteScore 2017: 1.45

SCImago Journal Rank (SJR) 2017: 0.349
Source Normalized Impact per Paper (SNIP) 2017: 0.812

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2391-5420
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Volume 6, Issue 3

Issues

Volume 13 (2015)

2-pyrrolidone - capped Mn3O4 nanocrystals

Tevhide Özkaya / Abdulhadi Baykal / Muhammet Toprak
Published Online: 2008-08-11 | DOI: https://doi.org/10.2478/s11532-008-0041-4

Abstract

Water-soluble Mn3O4 nanocrystals have been prepared through thermal decomposition in a high temperature boiling solvent, 2-pyrrolidone. The final product was characterized with XRD, SEM, TEM, FTIR and Zeta Potential measurements. Average crystallite size was calculated as ∼15 nm using XRD peak broadening. TEM analysis revealed spherical nanoparticles with an average diameter of 14±0.4 nm. FTIR analysis indicated that 2-pyrrolidone coordinates with the Mn3O4 nanocrystals only via O from the carbonyl group, thus confining their growth and protecting their surfaces from interaction with neighboring particles.

Keywords: Spinels; Nanocrystalline Materials; Thermal Decomposition; Mn3O4; Transmission Electron Microscopy (TEM)

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About the article

Published Online: 2008-08-11

Published in Print: 2008-09-01


Citation Information: Open Chemistry, Volume 6, Issue 3, Pages 465–469, ISSN (Online) 2391-5420, DOI: https://doi.org/10.2478/s11532-008-0041-4.

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© 2008 Versita Warsaw. This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License. BY-NC-ND 3.0

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