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Open Chemistry

formerly Central European Journal of Chemistry


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Volume 7, Issue 3

Issues

Volume 13 (2015)

Dispersive liquid-liquid microextraction and liquid chromatographic determination of pentachlorophenol in water

Khalil Farhadi / Mir Farajzadeh / Amir Matin
  • Department of Chemistry, Faculty of Science, Urmia University, Urmia, Iran
  • Research Department of Chromatography, Iranian Academic Center for Education, Culture & Research (ACECR), Urmia, Iran
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/ Paria Hashemi
  • Department of Chemistry, Faculty of Science, Urmia University, Urmia, Iran
  • Research Department of Chromatography, Iranian Academic Center for Education, Culture & Research (ACECR), Urmia, Iran
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Published Online: 2009-06-21 | DOI: https://doi.org/10.2478/s11532-009-0013-3

Abstract

A simple and sensitive dispersive liquid-liquid microextraction method for extraction and preconcentration of pentachlorophenol (PCP) in water samples is presented. After adjusting the sample pH to 3, extraction was performed in the presence of 1% W/V sodium chloride by injecting 1 mL acetone as disperser solvent containing 15 μL tetrachloroethylene as extraction solvent. The proposed DLLME method was followed by HPLC-DAD for determination of PCP. It has good linearity (0.994) with wide linear dynamic range (0.1–1000 μg L−1) and low detection limit (0.03 μg L−1), which makes it suitable for determination of PCP in water samples.

Keywords: Dispersive liquid-liquid microextraction; Herbicide; Pentachlorophenol; Water sample; High performance liquid chromatography

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About the article

Published Online: 2009-06-21

Published in Print: 2009-09-01


Citation Information: Open Chemistry, Volume 7, Issue 3, Pages 369–374, ISSN (Online) 2391-5420, DOI: https://doi.org/10.2478/s11532-009-0013-3.

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© 2009 Versita Warsaw. This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License. BY-NC-ND 3.0

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