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Open Chemistry

formerly Central European Journal of Chemistry


IMPACT FACTOR 2017: 1.425
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2391-5420
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Volume 7, Issue 3

Issues

Volume 13 (2015)

Sol-gel bioactive glass-ceramics Part I: Calcium phosphate silicate/wollastonite glass-ceramics

Lachezar Radev / Vladimir Hristov / Irena Michailova / Bisserka Samuneva
Published Online: 2009-06-21 | DOI: https://doi.org/10.2478/s11532-009-0022-2

Abstract

In this work we present experimental results about synthesis, structure evolution and in vitro bioactivity of new calcium phosphate silicate/wollastonite (CPS/W) glass-ceramics. The samples obtained were synthesized via polystep sol-gel process with different Ca/P+Si molar ratio (R). The structure of the materials obtained was studied by XRD, FTIR spectroscopy and SEM. XRD showed the presence of Ca15(PO4)2(SiO4)6, β-CaSiO3 and α-CaSiO3 for the sample with R=1.89 after thermal treatment at 1200°C/2h. The XRD results are in good agreement with FTIR analysis. SEM denotes that apatite formation can be observed after soaking in simulated body fluid (SBF).

Keywords: Sol-gel; Glass-ceramics; In vitro bioactivity

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About the article

Published Online: 2009-06-21

Published in Print: 2009-09-01


Citation Information: Open Chemistry, Volume 7, Issue 3, Pages 317–321, ISSN (Online) 2391-5420, DOI: https://doi.org/10.2478/s11532-009-0022-2.

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© 2009 Versita Warsaw. This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License. BY-NC-ND 3.0

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