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Open Chemistry

formerly Central European Journal of Chemistry


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Volume 7, Issue 3

Issues

Volume 13 (2015)

A green chemical route for the synthesis of Mn3O4 nanoparticles

Zehra Durmus / Hüseyin Kavas / Abdulhadi Baykal / Muhammet Toprak
Published Online: 2009-06-21 | DOI: https://doi.org/10.2478/s11532-009-0049-4

Abstract

A novel environmental friendly, room temperature route using an ionic liquid 1-n-butyl-3-methylimidazolium hydroxide ([BMIM]OH) for the synthesis of Mn3O4 nanoparticles is presented. The product was characterized using Fourier transform infrared spectroscopy, X-ray powder diffraction, and transmission electron microscopy. Phase purity was confirmed by XRD, and X-ray line profile fitting determined a crystallite size of 42 ± 11 nm. TEM analysis revealed various morphologies. EPR measurements have indicated the existence of long-range interactions, due to the wide range of particle sizes and morphologies observed.

Keywords: Ionic liquids; Nanoparticles; Mn3O4; [BMIM]OH; TEM; EPR

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About the article

Published Online: 2009-06-21

Published in Print: 2009-09-01


Citation Information: Open Chemistry, Volume 7, Issue 3, Pages 555–559, ISSN (Online) 2391-5420, DOI: https://doi.org/10.2478/s11532-009-0049-4.

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© 2009 Versita Warsaw. This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License. BY-NC-ND 3.0

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