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High Temperature Materials and Processes

Editor-in-Chief: Fukuyama, Hiroyuki

Editorial Board: Waseda, Yoshio / Fecht, Hans-Jörg / Reddy, Ramana G. / Manna, Indranil / Nakajima, Hideo / Nakamura, Takashi / Okabe, Toru / Ostrovski, Oleg / Pericleous, Koulis / Seetharaman, Seshadri / Straumal, Boris / Suzuki, Shigeru / Tanaka, Toshihiro / Terzieff, Peter / Uda, Satoshi / Urban, Knut / Baron, Michel / Besterci, Michael / Byakova, Alexandra V. / Gao, Wei / Glaeser, Andreas / Gzesik, Z. / Hosson, Jeff / Masanori, Iwase / Jacob, Kallarackel Thomas / Kipouros, Georges / Kuznezov, Fedor


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Open Access
Online
ISSN
2191-0324
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Volume 31, Issue 6

Issues

Synthesis of Different Morphologies of PbS Nanostructures via Hydrothermal Process

Davood Ghanbari / Masoud Salavati-Niasari
  • Corresponding author
  • Institute of Nano Science and Nano Technology, University of Kashan, Kashan, I. R. Iran
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
/ Fatemeh Davar
  • Department of Inorganic Chemistry, Faculty of Chemistry, Razi University, Kermanshah, I. R. Iran
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
Published Online: 2012-12-13 | DOI: https://doi.org/10.1515/htmp-2011-0152

Abstract

Lead sulfide nanostructures with different morphologies and particle sizes were obtained via a simple hydrothermal reaction between lead salicylate (Pb(Hsal)2) and thioglycolic acid The novelty in this synthesis is using of thioglycolic acid as a sulfur source and stability agent simultaneously. Depending on the pH of the solution, morphologies of the PbS varied and crystals with shapes of nanoparticles, flower-like nanostructures and microrods were obtained. The effect of the reaction time on the morphology of the nanostructures has been investigated. Products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) ultraviolet-visible (UV-vis) and Fourier transform infrared (FT-IR) spectroscopy.

Keywords: PbS; nanoparticles; hydrothermal

About the article

Institute of Nano Science and Nano Technology, University of Kashan, Kashan, P. O. Box. 87317–51167, I. R. Iran


Received: 2011-12-24

Accepted: 2012-02-18

Published Online: 2012-12-13

Published in Print: 2012-12-14


Citation Information: , Volume 31, Issue 6, Pages 707–710, ISSN (Online) 2191-0324, ISSN (Print) 0334-6455, DOI: https://doi.org/10.1515/htmp-2011-0152.

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Ceramics International, 2014, Volume 40, Number 6, Page 8143

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