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High Temperature Materials and Processes

Editor-in-Chief: Fukuyama, Hiroyuki

Editorial Board: Waseda, Yoshio / Fecht, Hans-Jörg / Reddy, Ramana G. / Manna, Indranil / Nakajima, Hideo / Nakamura, Takashi / Okabe, Toru / Ostrovski, Oleg / Pericleous, Koulis / Seetharaman, Seshadri / Straumal, Boris / Suzuki, Shigeru / Tanaka, Toshihiro / Terzieff, Peter / Uda, Satoshi / Urban, Knut / Baron, Michel / Besterci, Michael / Byakova, Alexandra V. / Gao, Wei / Glaeser, Andreas / Gzesik, Z. / Hosson, Jeff / Masanori, Iwase / Jacob, Kallarackel Thomas / Kipouros, Georges / Kuznezov, Fedor


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Open Access
Online
ISSN
2191-0324
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Volume 31, Issue 6

Issues

Facile Hydrothermal Synthesis of CoSO4ċH2O Nanoparticles and Barite Microcubes from Novel Precursors

Azam Sobhani
  • Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, I. R. Iran
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
/ Masoud Salavati-Niasari
Published Online: 2012-12-13 | DOI: https://doi.org/10.1515/htmp-2011-0153

Abstract

CoSO4ċH2O nanoparticles and barite (BaSO4) microcubes have been prepared by hydrothermal decomposition of new precursors [Co(tsc)2]Cl2 and [Ba(tsc)2]Cl2 (tsc =  thiosemicarbazide), respectively. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and Fourier transform infrared (FT-IR) spectroscopy. As a comparison between two methods, thermal decomposition of novel precursors in high temperature boiling organic solvents were examined.

Keywords: Nanoparticles; CoSO4ċH2O; BaSO4; hydrothermal; single-source precursor; thiosemicarbazide

About the article

Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, P. O. Box. 87317–51167, I. R. Iran


Received: 2011-12-24

Accepted: 2012-01-20

Published Online: 2012-12-13

Published in Print: 2012-12-14


Citation Information: , Volume 31, Issue 6, Pages 711–715, ISSN (Online) 2191-0324, ISSN (Print) 0334-6455, DOI: https://doi.org/10.1515/htmp-2011-0153.

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[2]
Masoud Salavati-Niasari, Azam Sobhani, Sanaz khoshrooz, and Noshin Mirzanasiri
Journal of Cluster Science, 2014, Volume 25, Number 4, Page 937

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