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Metrology and Measurement Systems

The Journal of Committee on Metrology and Scientific Instrumentation of Polish Academy of Sciences

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IMPACT FACTOR 2016: 1.598

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2300-1941
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Volume 24, Issue 1 (Mar 2017)

Examination of Sol-Gel Derived Hydroxyapatite Enhanced with Silver Nanoparticles using OCT and Raman Spectroscopy

Maciej J. Głowacki
  • 1) Gdańsk University of Technology, Faculty of Electronics, Telecommunications and Informatics, G. Narutowicza 11/12, 80-233 Gdańsk, Poland
  • 3) Gdańsk University of Technology, Faculty of Mechanical Engineering, G. Narutowicza 11/12, 80-233 Gdańsk, Poland
  • Email:
/ Marcin Gnyba
  • 1) Gdańsk University of Technology, Faculty of Electronics, Telecommunications and Informatics, G. Narutowicza 11/12, 80-233 Gdańsk, Poland
  • Email:
/ Paulina Strąkowska
  • 1) Gdańsk University of Technology, Faculty of Electronics, Telecommunications and Informatics, G. Narutowicza 11/12, 80-233 Gdańsk, Poland
  • 3) Gdańsk University of Technology, Faculty of Mechanical Engineering, G. Narutowicza 11/12, 80-233 Gdańsk, Poland
  • Email:
/ Mateusz Gardas
  • 2) Mateusz Gardas GAROCIN LABS, Świerkowa 4, 76-200 Słupsk, Poland
  • Email:
/ Maciej Kraszewski
  • 1) Gdańsk University of Technology, Faculty of Electronics, Telecommunications and Informatics, G. Narutowicza 11/12, 80-233 Gdańsk, Poland
  • Email:
/ Michał Trojanowski
  • 1) Gdańsk University of Technology, Faculty of Electronics, Telecommunications and Informatics, G. Narutowicza 11/12, 80-233 Gdańsk, Poland
  • Email:
/ Marcin R. Strąkowski
  • Corresponding author
  • 1) Gdańsk University of Technology, Faculty of Electronics, Telecommunications and Informatics, G. Narutowicza 11/12, 80-233 Gdańsk, Poland
  • Email:
Published Online: 2017-03-20 | DOI: https://doi.org/10.1515/mms-2017-0008

Abstract

Hydroxyapatite (HAp) has been attracting widespread interest in medical applications. In a form of coating, it enables to create a durable bond between an implant and surrounding bone tissues. With addition of silver nanoparticles HAp should also provide antibacterial activity. The aim of this research was to evaluate the composition of hydroxyapatite with silver nanoparticles in a non-destructive and non-contact way. For control measurements of HAp molecular composition and solvent evaporation efficiency the Raman spectroscopy has been chosen. In order to evaluate dispersion and concentration of the silver nanoparticles inside the hydroxyapatite matrix, the optical coherence tomography (OCT) has been used. Five samples were developed and examined ‒ a reference sample of pure HAp sol and four samples of HAp colloids with different silver nanoparticle solution volume ratios. The Raman spectra for each solution have been obtained and analyzed. Furthermore, a transverse-sectional visualization of every sample has been created and examined by means of OCT.

Keywords: hydroxyapatite; sol-gel; nanoparticles; Raman spectroscopy; optical coherence tomography (OCT)

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About the article

Received: 2016-07-27

Accepted: 2016-09-24

Published Online: 2017-03-20

Published in Print: 2017-03-01


Citation Information: Metrology and Measurement Systems, ISSN (Online) 2300-1941, DOI: https://doi.org/10.1515/mms-2017-0008.

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© 2017 Polish Academy of Sciences. This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License. BY-NC-ND 3.0

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