Jump to ContentJump to Main Navigation
Show Summary Details
More options …

Materials Science-Poland

4 Issues per year


IMPACT FACTOR 2016: 0.610

CiteScore 2016: 0.64

SCImago Journal Rank (SJR) 2015: 0.226
Source Normalized Impact per Paper (SNIP) 2015: 0.431

Open Access
Online
ISSN
2083-134X
See all formats and pricing
More options …

Combustion synthesis process for the rapid preparation of high-purity SrO powders

Francisco Granados-Correa
  • Departamento de Química, Instituto Nacional de Investigaciones Nucleares, A.P. 18-1027, Col. Escandón, Delegación Miguel Hidalgo., C.P. 11801, México, D.F., México
  • Email
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
/ Juan Bonifacio-Martínez
  • Departamento de Química, Instituto Nacional de Investigaciones Nucleares, A.P. 18-1027, Col. Escandón, Delegación Miguel Hidalgo., C.P. 11801, México, D.F., México
  • Email
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
Published Online: 2014-12-19 | DOI: https://doi.org/10.2478/s13536-014-0250-9

Abstract

A rapid, safe and simple technique for the production of high purity strontium oxide powders via a chemical combustion process is reported. The combustion reactions were performed to optimize the fuel to oxidizer ratios in the reaction mixtures required to obtain pure SrO powders by varying the molar ratio of chemical precursors and the temperature. The synthesized powders were characterized by X-ray diffraction, scanning electron microscopy, energy dispersive X-ray spectrometry, infrared spectroscopy, differential scanning calorimetry, thermogravimetric analysis, and N2-physisorption measurements. The results indicate that crystalline SrO was obtained using a 1:1 strontium nitrate: urea molar ratio at 1000 °C after 5 minutes. In addition, high-purity, homogeneous and crystalline SrO powders were easily produced in a short time via a chemical combustion process.

Keywords: strontium oxide; chemical combustion; XRD; IR spectral analysis; thermal analysis

  • [1] Yu J., Guo H., Cheng B., J. Solid State Chem., 179 (2006), 800. http://dx.doi.org/10.1016/j.jssc.2005.12.001CrossrefGoogle Scholar

  • [2] Li S., Zhang H., Xu J., Yang D., Mater. Lett., 59 (2005), 420. http://dx.doi.org/10.1016/j.matlet.2004.09.037CrossrefGoogle Scholar

  • [3] Yoosuk B., Krasae P., Puttasawat B., Udomsap P., Viriya-Empikul N., Faungnawakij K., Chem. Eng. J., 162 (2010), 58. http://dx.doi.org/10.1016/j.cej.2010.04.057CrossrefGoogle Scholar

  • [4] Joyce A.O., Strontium, Minerals Yearbook. Volume 1. Metals and Minerals, US, Bureau of Mines, 1992, 11323. Google Scholar

  • [5] Ozuna O., Hirata G.A., Kittrick M.C., J. Phys.-Condens. Mat., 16 (2004), 2585. http://dx.doi.org/10.1088/0953-8984/16/15/010CrossrefGoogle Scholar

  • [6] Chandrappa K.G., Venkatesha T.V., Nayana K.O., Punithkumar M.K., Mater. Corros., 63 (2012), 445. http://dx.doi.org/10.1002/maco.201005966CrossrefGoogle Scholar

  • [7] Kingsley J.J., Pederson L.R., Mater. Lett., 18 (1993), 89. http://dx.doi.org/10.1016/0167-577X(93)90063-4CrossrefGoogle Scholar

  • [8] Chandran R.G., Patil K.C., Mater. Lett., 10 (1990), 291. http://dx.doi.org/10.1016/0167-577X(90)90035-KCrossrefGoogle Scholar

  • [9] Manoharan S.S., Patil K.C., J. Am. Ceram. Soc., 75 (1992), 1012. http://dx.doi.org/10.1111/j.1151-2916.1992.tb04177.xCrossrefGoogle Scholar

  • [10] Li F., Hu, J. L., Zhang L.D., Chen G., J. Nucl. Mater., 300 (2002), 82. http://dx.doi.org/10.1016/S0022-3115(01)00710-3CrossrefGoogle Scholar

  • [11] Patil K.C., Aruna S.T., Mimami T., Curr. Opin. Solid St. M., 6(6) (2002), 507. http://dx.doi.org/10.1016/S1359-0286(02)00123-7CrossrefGoogle Scholar

  • [12] Biamino S., Badini C., J. Eur. Ceram. Soc., 24 (2004), 3021. http://dx.doi.org/10.1016/j.jeurceramsoc.2003.10.005CrossrefGoogle Scholar

  • [13] Chick L.A., Pederson L.R., Maupin G.D., Bates J.L., Thomas L.E., Exarhos G.H., Mater. Lett., 10 (1990), 6. http://dx.doi.org/10.1016/0167-577X(90)90003-5CrossrefGoogle Scholar

  • [14] Sharma S.K., Pitale S.S., Malik P.M., Dubey R.N., Qureshi M.S., Ojha S., Physica B, 405 (2010), 866. http://dx.doi.org/10.1016/j.physb.2009.10.005CrossrefGoogle Scholar

  • [15] Granados-Correa F., Bonifacio-Martínez J., Lara V.H., Bosch P., Bulbulian S., Appl. Surf. Sci., 254 (2008), 4688. http://dx.doi.org/10.1016/j.apsusc.2008.01.074CrossrefGoogle Scholar

  • [16] Alvarado-Ibarra Y., Granados-Correa F., Lara V.H., Bosch P., Bulbulian S., Colloid. Surface A, 345 (2009), 135. http://dx.doi.org/10.1016/j.colsurfa.2009.04.045CrossrefGoogle Scholar

  • [17] Granados-Correa F., Jiménez-Reyes M., Sep. Sci. Technol., 46 (2011), 2360. http://dx.doi.org/10.1080/01496395.2011.595754CrossrefGoogle Scholar

  • [18] Medine G.M., Klabunde K.J., Zaikovskii V., J. Nanopart. Res., 4 (2002), 357. http://dx.doi.org/10.1023/A:1021168927908CrossrefGoogle Scholar

  • [19] Mathews T., Subasri R., Sreedharan O.M., Solid State Ionics, 148 (2002), 135. http://dx.doi.org/10.1016/S0167-2738(02)00105-4CrossrefGoogle Scholar

  • [20] Cruz D., Pfeiffer H., Bulbulian S., Solid State Sci., 8 (2006), 470. http://dx.doi.org/10.1016/j.solidstatesciences.2006.01.003CrossrefGoogle Scholar

  • [21] Campbell P.F., Ortner M.H., Anderson C., Anal. Chem., 33 (1961), 58. http://dx.doi.org/10.1021/ac60169a016CrossrefGoogle Scholar

  • [22] Sahu R.K., Ray A.K., Das S.K., Kailath A.J., Pathak L.C., J. Mater. Res., 21 (2006), 1664. http://dx.doi.org/10.1557/jmr.2006.0211CrossrefGoogle Scholar

  • [23] Lowell S., Introduction to Powder Surface Area, Interscience Publishers, Toronto, Canada, 1979. Google Scholar

About the article

Published Online: 2014-12-19

Published in Print: 2014-12-01


Citation Information: Materials Science-Poland, ISSN (Online) 2083-134X, DOI: https://doi.org/10.2478/s13536-014-0250-9.

Export Citation

© 2014 Wroclaw University of Technology. This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License. BY-NC-ND 3.0

Citing Articles

Here you can find all Crossref-listed publications in which this article is cited. If you would like to receive automatic email messages as soon as this article is cited in other publications, simply activate the “Citation Alert” on the top of this page.

[1]
Gutiérrez-Bonilla Elvira, Granados-Correa Francisco, Sánchez-Mendieta Víctor, and Morales-Luckie Raúl Alberto
Journal of Environmental Sciences, 2017, Volume 57, Page 418
[2]
Robert Ianoş, Roxana Istratie, Cornelia Păcurariu, and Radu Lazău
Phys. Chem. Chem. Phys., 2016, Volume 18, Number 2, Page 1150

Comments (0)

Please log in or register to comment.
Log in