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Pure and Applied Chemistry

The Scientific Journal of IUPAC

Ed. by Burrows, Hugh / Weir, Ron / Stohner, Jürgen

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1365-3075
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Volume 73, Issue 10 (Oct 2001)

Issues

Standards in isothermal microcalorimetry (IUPAC Technical Report)

Ingemar Wadsö
  • Corresponding author
  • Physical Chemistry 1, Chemical Center, University of Lund, P.O. Box 124, S-221 00 Lund, Sweden
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
/ Robert N. Goldberg
  • Corresponding author
  • Biotechnology Division, National Institute of Standards and Technology, Gaithersburg, MD 20899, USA
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  • De Gruyter OnlineGoogle Scholar
Published Online: 2009-01-01 | DOI: https://doi.org/10.1351/pac200173101625

The main calorimetric principles used in isothermal microcalorimetry are briefly discussed. Different chemical calibration and test reactions are discussed, with a focus on reactions suitable for ambient conditions: reactions initiated by mixing of liquids (including titration microcalorimetry), dissolution of solid compounds and of slightly soluble gases, a photochemical process, and thermal power signals released over an extended period of time. Guidelines on the use of standardized chemical test and calibration reactions in isothermal microcalorimetry are presented. A standardized terminology in reporting characteristics of isothermal microcalorimeters is proposed.

Project Year: 1997, Project Code: 120/18/97

About the article

Published Online: 2009-01-01

Published in Print: 2001-10-01


Citation Information: Pure and Applied Chemistry, ISSN (Online) 1365-3075, ISSN (Print) 0033-4545, DOI: https://doi.org/10.1351/pac200173101625.

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Russian Chemical Bulletin, 2007, Volume 56, Number 4, Page 739
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Journal of Thermal Analysis and Calorimetry, 2007, Volume 89, Number 3, Page 841
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