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Pure and Applied Chemistry

The Scientific Journal of IUPAC

Ed. by Burrows, Hugh / Weir, Ron / Stohner, Jürgen

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Standards in isothermal microcalorimetry (IUPAC Technical Report)

Ingemar Wadsö
  • Physical Chemistry 1, Chemical Center, University of Lund, P.O. Box 124, S-221 00 Lund, Sweden
/ Robert N. Goldberg
  • Biotechnology Division, National Institute of Standards and Technology, Gaithersburg, MD 20899, USA
Published Online: 2009-01-01 | DOI: https://doi.org/10.1351/pac200173101625

The main calorimetric principles used in isothermal microcalorimetry are briefly discussed. Different chemical calibration and test reactions are discussed, with a focus on reactions suitable for ambient conditions: reactions initiated by mixing of liquids (including titration microcalorimetry), dissolution of solid compounds and of slightly soluble gases, a photochemical process, and thermal power signals released over an extended period of time. Guidelines on the use of standardized chemical test and calibration reactions in isothermal microcalorimetry are presented. A standardized terminology in reporting characteristics of isothermal microcalorimeters is proposed.

Project Year: 1997, Project Code: 120/18/97


Published Online: 2009-01-01

Published in Print: 2001-10-01


Citation Information: Pure and Applied Chemistry. Volume 73, Issue 10, Pages 1625–1639, ISSN (Online) 1365-3075, ISSN (Print) 0033-4545, DOI: https://doi.org/10.1351/pac200173101625, January 2009

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