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Pure and Applied Chemistry

The Scientific Journal of IUPAC

Ed. by Burrows, Hugh / Weir, Ron / Stohner, Jürgen

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1365-3075
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Volume 73, Issue 8

Issues

Solvent-free preparation of ionic liquids using a household microwave oven

Rajender S. Varma
  • Corresponding author
  • Clean Processes Branch, National Risk Management Research Laboratory, U.S. Environmental Protection Agency, MS 443, 26 W. Martin Luther King Drive, Cincinnati, OH 45268, USA
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
/ Vasudevan V. Namboodiri
  • Corresponding author
  • Clean Processes Branch, National Risk Management Research Laboratory, U.S. Environmental Protection Agency, MS 443, 26 W. Martin Luther King Drive, Cincinnati, OH 45268, USA
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
Published Online: 2009-01-01 | DOI: https://doi.org/10.1351/pac200173081309

An efficient solventless protocol for the preparation of a wide variety of ionic liquids is described, which requires a simple exposure of admixed 1-methylimidazole and alkyl halides to microwave irradiation in open glass containers. The details of this clean process using a common household microwave oven, which exploits the newer inverter technology system for better power attenuation, are described. The characterization and thermal stability data on selected ionic liquids and their potential applications are summarized.

Conference

IUPAC CHEMRAWN XIV Conference on Green Chemistry:Toward Environmentally Benign Processes and Products, Chemical Research Applied To World Needs, CHEMRAWN, Chemical Research Applied To World Needs, Boulder, Colorado, USA, 2001-06-09–2001-06-13

About the article

Published Online: 2009-01-01

Published in Print: 2001-08-01


Citation Information: Pure and Applied Chemistry, Volume 73, Issue 8, Pages 1309–1313, ISSN (Online) 1365-3075, ISSN (Print) 0033-4545, DOI: https://doi.org/10.1351/pac200173081309.

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