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Pure and Applied Chemistry

The Scientific Journal of IUPAC

Ed. by Burrows, Hugh / Weir, Ron / Stohner, Jürgen

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Online
ISSN
1365-3075
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In This Section
Volume 76, Issue 9 (Sep 2004)

Issues

Design of composite micro/mesoporous molecular sieve catalysts

I. I. Ivanova
  • Corresponding author
  • Department of Chemistry, Moscow State University, Lenin Hills, Moscow 119992, Russia
/ A. S. Kuznetsov
  • Corresponding author
  • Department of Chemistry, Moscow State University, Lenin Hills, Moscow 119992, Russia
/ V. V. Yuschenko
  • Corresponding author
  • Department of Chemistry, Moscow State University, Lenin Hills, Moscow 119992, Russia
/ E. E. Knyazeva
  • Corresponding author
  • Department of Chemistry, Moscow State University, Lenin Hills, Moscow 119992, Russia
Published Online: 2009-01-01 | DOI: https://doi.org/10.1351/pac200476091647

Two series of composite micro/mesoporous materials with different contributions of micro- and mesoporosity were prepared by dealumination and recrystallization of mordenite zeolite. The materials were characterized by X-ray diffraction, infrared spectroscopy, 27Al magic angle spinning (MAS) NMR, nitrogen adsorption–desorption, and temperature-programmed desorption of ammonia (TPD NH3). Catalytic properties were studied in transalkylation of biphenyl with diisopropylbenzene. Both types of composite materials showed remarkably high activity, stability, and selectivity toward formation of di-isopropylbiphenyls with respect to both pure microporous and mesoporous materials. The effect is due to high zeolitic acidity combined with improved accessibility of active sites and transport of bulky molecules provided by mesopores.

Conference

Mendeleev Congress on General and Applied Chemistry, XVII, Kazan, Tatarstan, Russia, 2003-09-21–2003-09-26

About the article

Published Online: 2009-01-01

Published in Print: 2004-09-30



Citation Information: Pure and Applied Chemistry, ISSN (Online) 1365-3075, ISSN (Print) 0033-4545, DOI: https://doi.org/10.1351/pac200476091647. Export Citation

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