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Pure and Applied Chemistry

The Scientific Journal of IUPAC

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Volume 78, Issue 7 (Jan 2006)

Issues

Standards, calibration, and guidelines in microcalorimetry. Part 2. Calibration standards for differential scanning calorimetry* (IUPAC Technical Report)

Giuseppe Della Gatta
  • Corresponding author
  • Department of Chemistry IFM, University of Turin, Via P. Giuria 9, 10125 Torino, Italy
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/ Michael J. Richardson
  • Corresponding author
  • Polymer Research Centre, University of Surrey, Guildford GU2 5XH, Surrey, UK
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/ Stefan M. Sarge
  • Corresponding author
  • Physikalisch-Technische Bundesanstalt, Bundesallee 100, 38116 Braunschweig, Germany
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/ Svein Stølen
  • Corresponding author
  • Department of Chemistry, University of Oslo, P.O. Box 1033, Blindern, 0315 Oslo, Norway
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Published Online: 2009-01-01 | DOI: https://doi.org/10.1351/pac200678071455

Differential scanning calorimeters (DSCs) are widely used for temperature, heat capacity, and enthalpy measurements in the range from subambient to high temperatures. The present recommendations describe procedures and reference materials (RMs) for the calibration of DSCs. The recommendations focus on the calibration of the response of the instrument and on the estimation of the measurement uncertainty. The procedures for temperature, enthalpy, and heat-flow rate calibration are given in detail. Calibration on cooling has also been considered. Recommended RMs are listed, and the relevant properties of these materials are discussed.

Keywords: DSC; enthalpy measurements; heat capacity; IUPAC Physical and Biophysical Chemistry Division; microcalorimetry

Project Year: 1997, Project Code: 120/18/97

About the article

Published Online: 2009-01-01

Published in Print: 2006-01-01


Citation Information: Pure and Applied Chemistry, ISSN (Online) 1365-3075, ISSN (Print) 0033-4545, DOI: https://doi.org/10.1351/pac200678071455.

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