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Zeitschrift für Kristallographie - Crystalline Materials

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Ed. by Antipov, Evgeny / Bismayer, Ulrich / Boldyreva, Elena V. / Huppertz, Hubert / Petrícek, Václav / Tiekink, E. R. T.

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Die Molekular- und Kristallstruktur von 4-Methoxy-6-(l′,2′-dihydrostyryl)-5,6-dihydro-α-pyron (Dihydrokavain) C14H16O3*

P. Engel / W. Nowacki

Citation Information: Zeitschrift für Kristallographie. Volume 136, Issue 5-6, Pages 453–467, ISSN (Online) 0044-2968, ISSN (Print) 1433-7266, DOI: https://doi.org/10.1524/zkri.1972.136.5-6.453, July 2010

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The crystalline form of 4-methoxy-6-(1′,2′-dihydrostyryl)-5,6-dihydro-α-pyrone is assigned to space group P21/cC2h5 having parameters a = 10.921, b = 7.605, c = 17.014 Å and β = 119°30′. The crystal structure was found by phase assignment with the symbolic-addition procedure. The resulting E map showed the whole molecule. The refinement by the block-diagonal-matrix least squares led to a R value of 0.09 using 2352 reflections. A short discussion of the structure is given.

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