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Zeitschrift für Kristallographie - Crystalline Materials

Editor-in-Chief: Pöttgen, Rainer

Ed. by Antipov, Evgeny / Bismayer, Ulrich / Boldyreva, Elena V. / Huppertz, Hubert / Petrícek, Václav / Tiekink, E. R. T.

12 Issues per year


IMPACT FACTOR 2016: 3.179

CiteScore 2016: 3.30

SCImago Journal Rank (SJR) 2016: 1.097
Source Normalized Impact per Paper (SNIP) 2016: 2.592

Online
ISSN
2196-7105
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Volume 169, Issue 1-4 (Jan 1984)

Issues

Crystal and molecular structure of hexa(antipyrine)cadmium(II) perchlorate, [(C11H12ON2)6Cd]2+ [ClO4]2

C. Mahadevan / Akella Radha / M. Seshasayee
Published Online: 2010-08-25 | DOI: https://doi.org/10.1524/zkri.1984.169.1-4.159

Abstract

The crystal and molecular structure of the title compound is reported. Crystals are trigonal with hexagonal axes, space group P[unk] with Z = 1 in a unit cell of dimensions a = b = 14.196(7) and c = 9.558(5) Å. The structure was solved by the heavy-atom method and refined by the full-matix least-squares method to R = 0.071 for 1097 unique reflections. The metal atom of the cation has a regular octahedral configuration and the chlorine atoms of the anions have regular tetrahedral configuration. Both the five- and six-membered rings in the antipyrine are planar having an angle of 113° between the normals to their planes.

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Published Online: 2010-08-25

Published in Print: 1984


Citation Information: Zeitschrift für Kristallographie, ISSN (Online) 0044-2968, ISSN (Print) 1433-7266, DOI: https://doi.org/10.1524/zkri.1984.169.1-4.159.

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