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Zeitschrift für Kristallographie - Crystalline Materials

Editor-in-Chief: Pöttgen, Rainer

Ed. by Antipov, Evgeny / Bismayer, Ulrich / Boldyreva, Elena V. / Huppertz, Hubert / Petrícek, Václav / Tiekink, E. R. T.

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Rank 8 out of 26 in category Cristallography in the 2015 Thomson Reuters Journal Citation Report/Science Edition

SCImago Journal Rank (SJR) 2015: 0.827
Source Normalized Impact per Paper (SNIP) 2015: 1.198
Impact per Publication (IPP) 2015: 1.834

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Crystal and molecular structure of hexa(antipyrine)cadmium(II) perchlorate, [(C11H12ON2)6Cd]2+ [ClO4]2

C. Mahadevan / Akella Radha / M. Seshasayee

Citation Information: Zeitschrift für Kristallographie. Volume 169, Issue 1-4, Pages 159–163, ISSN (Online) 0044-2968, ISSN (Print) 1433-7266, DOI: 10.1524/zkri.1984.169.1-4.159, August 2010

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The crystal and molecular structure of the title compound is reported. Crystals are trigonal with hexagonal axes, space group P[unk] with Z = 1 in a unit cell of dimensions a = b = 14.196(7) and c = 9.558(5) Å. The structure was solved by the heavy-atom method and refined by the full-matix least-squares method to R = 0.071 for 1097 unique reflections. The metal atom of the cation has a regular octahedral configuration and the chlorine atoms of the anions have regular tetrahedral configuration. Both the five- and six-membered rings in the antipyrine are planar having an angle of 113° between the normals to their planes.

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