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Zeitschrift für Kristallographie - Crystalline Materials

Editor-in-Chief: Pöttgen, Rainer

Ed. by Antipov, Evgeny / Boldyreva, Elena V. / Friese, Karen / Huppertz, Hubert / Jahn, Sandro / Tiekink, E. R. T.

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CiteScore 2017: 2.65

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2196-7105
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Volume 210, Issue 11

Issues

Crystal structure modulations in η-Cu5Sn4

A.-K. Larsson / L. Stenberg / S. Lidin
Published Online: 2010-07-28 | DOI: https://doi.org/10.1524/zkri.1995.210.11.832

Abstract

The high temperature modification of η-Cu6Sn5 (reassigned η-Cu5Sn4) was by means of electron diffraction found to exhibit structural modulations. The diffraction patterns may be indexed using the basic NiAs-cell and a modulation vector q ≈ (δa*/24, δa*/24, c*/2), 8 ≤ δ ≤ 9. Models for the crystal structures of the two commensurate modulations δ = 8 and δ = 9 are suggested. Both superstructures are caused by the ordered occupancy of Cu in the trigonal bipyramidal sites. The model given for η6-Cu5Sn4 (corresponding to δ = 8, found above 350° C) has the space group C2 and cell parameters a = 12.60 Å, b = 7.27 Å and c = 10.20 Å and β = 90.0°. η8-Cu5Sn4, corresponding to δ = 9, has the unit cell (in P21/c) a = c = 9.83 Å, b = 7.27 Å and β = 62.5°.

About the article

Published Online: 2010-07-28

Published in Print: 1995-11-01


Citation Information: Zeitschrift für Kristallographie - Crystalline Materials, Volume 210, Issue 11, Pages 832–837, ISSN (Online) 2196-7105, ISSN (Print) 2194-4946, DOI: https://doi.org/10.1524/zkri.1995.210.11.832.

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