Crystal chemistry of inorganic compounds based on chains of oxocentered tetrahedra

doi:10.1524/zkri.1998.213.12.645

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Zeitschrift für Kristallographie - Crystalline Materials

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I. Crystal structure of chloromenite, Cu₉O₂(SeO₃)₄Cl₆

S. V. Krivovichev / S. K. Filatov / T. F. Semenova / I. V. Rozhdestvenskaya

Published Online: 2010-07-28 | DOI: https://doi.org/10.1524/zkri.1998.213.12.645

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Abstract

The crystal structure of chloromenite, Cu₉O₂(SeO₃)₄Cl₆, a = 14.170(3) Å, b = 6.262(1) Å, c = 12.999(3) Å, β = 113.05(1)°, V = 1061.3(4) Å³, Z = 2, space group I2/m, has been solved by direct methods and refined to an R(F) index of 0.051 (wR(F²) = 0.128). The structure is based on unbranched zweier single chains {uB, 1¹_∞} [O₂Cu₆] of corner sharing [OCu₄] tetrahedra running parallel to the b axis. The geometry of structurally similar [uB, l¹_∞}[O₂M₆] (M = Cu, Zn) chains of oxocentered [OM₄] tetrahedra (M = Cu, Zn) in inorganic compounds is discussed.

About the article

Published Online: 2010-07-28

Published in Print: 1998-12-01

Citation Information: Zeitschrift für Kristallographie - Crystalline Materials, Volume 213, Issue 12, Pages 645–649, ISSN (Online) 2196-7105, ISSN (Print) 2194-4946, DOI: https://doi.org/10.1524/zkri.1998.213.12.645.

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Citing Articles

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[1]

Emulating exhalative chemistry: synthesis and structural characterization of ilinskite, Na[Cu5O2](SeO3)2Cl3, and its K-analogue

Vadim M. Kovrugin, Oleg I. Siidra, Marie Colmont, Olivier Mentré, and Sergey V. Krivovichev

Mineralogy and Petrology, 2015, Volume 109, Number 4, Page 421

DOI: 10.1007/s00710-015-0369-3

[2]

Anion-Centered Tetrahedra in Inorganic Compounds

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Chemical Reviews, 2013, Volume 113, Number 8, Page 6459

DOI: 10.1021/cr3004696

[3]

The crystal structure of ilinskite, NaCu5O2(SeO3)2Cl3, and review of mixed-ligand CuOmCln coordination geometries in minerals and inorganic compounds

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Mineralogy and Petrology, 2013, Volume 107, Number 2, Page 235

DOI: 10.1007/s00710-012-0238-2

[4]

Crystal structure of Pb3O2(OH)Br, a Br-analogue of damaraite

Sergey V. Krivovichev and Peter C. Burns

Solid State Sciences, 2001, Volume 3, Number 4, Page 455

DOI: 10.1016/S1293-2558(01)01163-3

[5]

Crystal structure and magnetic properties of Co7(TeO3)4Br6—a new cobalt tellurite bromide

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Solid State Sciences, 2006, Volume 8, Number 7, Page 836

DOI: 10.1016/j.solidstatesciences.2006.03.004

[6]

Cu3(SeO3)2Cl2: a new oxochloride of copper(II) and selenium(IV)

P. Millet, B. Bastide, and M. Johnsson

Solid State Communications, 2000, Volume 113, Number 12, Page 719

DOI: 10.1016/S0038-1098(99)00548-7

[7]

Synthesis of copper(II) and selenium(IV) oxochlorides by chemical transport reaction: crystal structure of Cu9O2(SeO3)4Cl6

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Materials Research Bulletin, 2000, Volume 35, Number 6, Page 847

DOI: 10.1016/S0025-5408(00)00279-8

[8]

Synthesis, crystal structure and magnetic property of a new nickel selenite chloride: Ni5(SeO3)4Cl2

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DOI: 10.1016/j.jssc.2005.07.005

[9]

Crystal chemistry of inorganic compounds based on chains of oxocentered tetrahedra III. Crystal structure of georgbokiite, Cu5O2(SeO3)2Cl21

S. V. Krivovichev, R. R. Shuvalov, T. F. Semenova, and S. K. Filatov

Zeitschrift für Kristallographie - Crystalline Materials, 1999, Volume 214, Number 3

DOI: 10.1524/zkri.1999.214.3.135

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