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Zeitschrift für Kristallographie - Crystalline Materials

Editor-in-Chief: Pöttgen, Rainer

Ed. by Antipov, Evgeny / Bismayer, Ulrich / Boldyreva, Elena V. / Friese, Karen / Huppertz, Hubert / Tiekink, E. R. T.

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Volume 218, Issue 6

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Hydroxy-alkyl bisphosphonic acid partial esters (HABPA-PE): Structures of two symmetrical and non-symmetrical members of a new class of prodrugs in bone disease treatments

C. Barbey / M. Lecouvey / I. Mallard / Th. Prangé / A. Neuman / M. Lance / A. Navaza
Published Online: 2009-09-25 | DOI: https://doi.org/10.1524/zkri.218.6.445.20719

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Abstract

Two new hydroxy alkyl bisphosphonate partial esters (HABPA-PE) have been crystallised. The first compound C6H15NaO7P2C2H5O, crystallises as an ethanol solvate and forms rigid infinite β-sheet-like ribbons. The second, C6H16O7P2, displays self-association in dimers. In these new structures, packing analyses confirm the enhanced hydrophobic character due to partial esterification compared to naked hydroxybisphosphonic acids and the simplification of their H bonding patterns.

About the article

Published Online: 2009-09-25

Published in Print: 2003-06-01

Citation Information: Zeitschrift für Kristallographie - Crystalline Materials, Volume 218, Issue 6, Pages 445–449, ISSN (Online) 2196-7105, ISSN (Print) 2194-4946, DOI: https://doi.org/10.1524/zkri.218.6.445.20719.

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[1]
Nathalie Dupont, Pascal Retailleau, Evelyne Migianu-Griffoni, and Carole Barbey
Acta Crystallographica Section E Structure Reports Online, 2008, Volume 64, Number 10, Page o1874

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