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Zeitschrift für Kristallographie - Crystalline Materials

Editor-in-Chief: Pöttgen, Rainer

Ed. by Antipov, Evgeny / Bismayer, Ulrich / Boldyreva, Elena V. / Friese, Karen / Huppertz, Hubert / Tiekink, E. R. T.

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2196-7105
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Volume 218, Issue 8

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The twinned and disordered crystal structure of tetrakis(triphenylphosphine)silver(I)bis(trifluoroacetato)triphenylstannate(IV)

Seik Weng Ng / A. David Rae
Published Online: 2009-09-25 | DOI: https://doi.org/10.1524/zkri.218.8.581.20690

Abstract

The crystal structure of tetrakis(triphenyl-phosphine)silver(I)bis(trifluoroacetato)triphenylstannate(IV), [(C6H5)3P]4Ag (C6H5)3Sn(O2CCF3)2 [R3: a = 16.238(1), c = 52.354(3) Å], consists of discrete four-coordinate te trahedral cations and five-coordinate trans-C3SnO2 trigonal bipramidal anions. The asymmetric unit consists of a third of each of two cations and two anions. The structure is a 0.675(3): 0.325 twin of a 0.783(1): 0.217 disorder of an R3 structure that uses a 2-fold rotation operation of R32 for the twinning and the disorder. The structure is refined on 234 variables and 6276 reflections with I > 3σ(I) to RF = 0.053.

About the article

Published Online: 2009-09-25

Published in Print: 2003-08-01


Citation Information: Zeitschrift für Kristallographie - Crystalline Materials, Volume 218, Issue 8, Pages 581–584, ISSN (Online) 2196-7105, ISSN (Print) 2194-4946, DOI: https://doi.org/10.1524/zkri.218.8.581.20690.

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