Synthesis, crystal structure, spectroscopic and thermal characterization of (Hampy)2[Ni(pydc)2(H2O)2] · 2 H2O

Alper Tolga Çolak; Demet Akduman; Okan Zafer Yesilel; Orhan Büyükgüngör

doi:10.1524/zkri.2009.1112

Show Summary Details

More options …

Zeitschrift für Kristallographie - Crystalline Materials

Editor-in-Chief: Pöttgen, Rainer

Ed. by Antipov, Evgeny / Bismayer, Ulrich / Boldyreva, Elena V. / Friese, Karen / Huppertz, Hubert / Tiekink, E. R. T.

12 Issues per year

IMPACT FACTOR 2016: 3.179

CiteScore 2017: 2.65

See all formats and pricing

Online
ISSN: 2196-7105

Online: Institutional Subscription
€ [D] 2213.00 / US$ 2988.00 / GBP 1815.00*
Individual Subscription
€ [D] 249.00 / US$ 374.00 / GBP 205.00*
Print: Institutional Subscription
€ [D] 2213.00 / US$ 2988.00 / GBP 1815.00*
Individual Subscription
€ [D] 2213.00 / US$ 2988.00 / GBP 1815.00*
Print + Online: Institutional Subscription
€ [D] 2629.00 / US$ 3548.00 / GBP 2155.00*
Individual Subscription
€ [D] 2506.00 / US$ 3383.00 / GBP 2055.00*

*Prices in US$ apply to orders placed in the Americas only. Prices in GBP apply to orders placed in Great Britain only. Prices in € represent the retail prices valid in Germany (unless otherwise indicated). Prices are subject to change without notice. Prices do not include postage and handling if applicable. RRP: Recommended Retail Price.

More options …

Ahead of print

Most Downloaded Articles
First principles methods using CASTEP by Clark, Stewart J./ Segall, Matthew D./ Pickard, Chris J./ Hasnip, Phil J./ Probert, Matt I. J./ Refson, Keith and Payne, Mike C.
The Rietveld Method: A Retrospection by Rietveld, H. M.
Classical vibrational modes in phononic lattices: theory and experiment by Sigalas, Mihail/ Kushwaha, Manvir S./ Economou, Eleftherios N./ Kafesaki, Maria/ Psarobas, Ioannis E. and Steurer, Walter
Structural chemistry of superconducting pnictides and pnictide oxides with layered structures by Johrendt, Dirk / Hosono, Hideo/ Hoffmann, Rolf-Dieter and Pöttgen, Rainer
SUMOF-5: a mesoporous metal-organic framework with the tbo topology built from the dicopper paddle-wheel cluster and a new tritopic linker by Yao, Qingxia/ Su, Jie and Zou, Xiaodong
Single-phase high-entropy alloys – an overview by Kozak, Roksolana/ Sologubenko, Alla and Steurer, Walter
Disputed discovery: The beginnings of X-ray diffraction in crystals in 1912 and its repercussions by Eckert, Michael
Simulation of crystal structures by a combined distance-least-squares/valence-rule method
Stacking disorders in zeolites and open-frameworks – structure elucidation and analysis by electron crystallography and X-ray diffraction by Willhammar, Tom and Zou, Xiaodong
The Mott insulators at extreme conditions; structural consequences of pressure-induced electronic transitions by Rozenberg, Gregory Kh./ Xu, Weiming and Pasternak, Moshe P.
High pressure neutron and X-ray diffraction at low temperatures by Ridley, Christopher J. and Kamenev, Konstantin V.
Structure determination of the intermediate tin oxide Sn3O4 by precession electron diffraction by White, Thomas A. / Moreno, M. Sergio and Midgley, Paul A.
Possibilities and limitations of parametric Rietveld refinement on high pressure data: The case study of LaFeO3 by Dinnebier/ Etter/ Müller and Hanfland
X-ray crystallography of simple molecular solids up to megabar pressures: application to solid oxygen and carbon dioxide by Datchi, Dr. Frédéric and Weck, Dr. Gunnar
Superconducting nitride halides MNX (M = Ti, Zr, Hf; X = Cl, Br, I) by Schurz, Christian M./ Shlyk, Larysa / Schleid, Thomas and Niewa, Rainer
Crystallography from Haüy to Laue: controversies on the molecular and atomistic nature of solids by Kubbinga, Henk
Multicomponent organic crystals at high pressure by Boldyreva
Correlation of structure, composition and local mechanical properties in the dorsal carapace of the edible crab Cancer pagurus by Fabritius, Helge-Otto/ Karsten, Eva Simone/ Balasundaram, Keerthika / Hild, Sabine/ Huemer, Katja and Raabe, Dierk
A crystal chemical approach to superconductivity. I. A bond-valence sum analysis of inorganic compounds by Liebau, Friedrich/ Klein, Hans-Joachim and Wang, Xiqu
MIL-53(Fe): a good example to illustrate the power of powder diffraction in the field of MOFs by Guillou, Nathalie/ Walton, R. I. and Millange, F.
Most Downloaded Articles

Submission of Manuscripts

Synthesis, crystal structure, spectroscopic and thermal characterization of (Hampy)₂[Ni(pydc)₂(H₂O)₂] · 2 H₂O

Alper Tolga Çolak / Demet Akduman

¹ Türkei
Other articles by this author:
De Gruyter Online Google Scholar

/ Okan Zafer Yesilel

² Ondokuz Mayis University, Department of Chemistry, Kurupelit, Samsun, Türkei
Other articles by this author:
De Gruyter Online Google Scholar

/ Orhan Büyükgüngör

³ Ondokuz Mayıs University, Department of Physics, Kurupelit, Samsun, Türkei
Other articles by this author:
De Gruyter Online Google Scholar

Published Online: 2009-09-25 | DOI: https://doi.org/10.1524/zkri.2009.1112

30,00 € / $42.00 / £23.00

Get Access to Full Text

Abstract

A supramolecular complex, bis(2-amino-3-methylpyridinium) diaquabis(pyridinedicarboxylato)nicke-late(II) dihydrate, (Hampy)₂[Ni(pydc)₂(H₂O)₂] · 2 H₂O (ampy = 2-amino-3-methylpyridine, H₂pydc = 2,5-pyridinedicarboxylic acid or isocinchomeronic acid) (1) has been prepared and characterized by elemental, spectral (IR and UV-vis.), thermal analysis, magnetic measurement and single crystal X-ray diffraction techniques. Ni(II) ion exhibits a distorted octahedral geometry coordinated by nitrogen and oxygen atoms of two pyridinedicarboxylate ligands, oxygen atoms from the two aqua ligands. The supramolecular network is constructed by N–H · · · O strong hydrogen bonds, π-π and C–H · · · π interactions.

Keywords: 2,5-pyridinedicarboxylic; 2-amino-3-methylpyridine; Nickel(II); Single crystal structure analysis; X-ray diffraction

About the article

^* Correspondence address: 43100 Kütahya, TURKEY,

Published Online: 2009-09-25

Published in Print: 2009-04-01

Citation Information: Zeitschrift für Kristallographie International journal for structural, physical, and chemical aspects of crystalline materials, Volume 224, Issue 4, Pages 207–212, ISSN (Print) 0044-2968, DOI: https://doi.org/10.1524/zkri.2009.1112.

Export Citation

Citing Articles

Here you can find all Crossref-listed publications in which this article is cited. If you would like to receive automatic email messages as soon as this article is cited in other publications, simply activate the “Citation Alert” on the top of this page.

[1]

The syntheses, crystal structures, spectroscopic and thermal characterization of new pyridine-2,5-dicarboxylate compounds

Deniz Doğan, Alper Tolga Çolak, Onur Şahin, Tuncay Tunç, and Ömer Çelik

Polyhedron, 2015, Volume 93, Page 37

DOI: 10.1016/j.poly.2015.03.033

[2]

Supramolecular Interactions between Finite Tapes of Water Molecules and Hydrated Metal Ions To Produce Infinite Two-Dimensional Cationic Layers of Water Molecules

Geeta Hundal, Maninder Singh Hundal, Young Kyu Hwang, and Jong San Chang

Crystal Growth & Design, 2014, Volume 14, Number 1, Page 172

DOI: 10.1021/cg401358p

[3]

Insight into the connecting roles of interaction synthons and water clusters within different transition metal coordination compounds of pyridine-2,5-dicarboxylic acid: experimental and theoretical studies

Hossein Eshtiagh-Hosseini, Masoud Mirzaei, Marzieh Biabani, Vito Lippolis, Mohammad Chahkandi, and Carla Bazzicalupi

CrystEngComm, 2013, Volume 15, Number 34, Page 6752

DOI: 10.1039/c3ce40743h

[4]

A two-dimensional photoluminescent cadmium(II) coordination polymer containing a new coordination mode of pyridine-2,3-dicarboxylate: Synthesis, structure and molecular simulations for gas storage and separation applications

Fatih Semerci, Okan Zafer Yeşilel, Mustafa Serkan Soylu, Seda Keskin, and Orhan Büyükgüngör

Polyhedron, 2013, Volume 50, Number 1, Page 314

DOI: 10.1016/j.poly.2012.10.009

[5]

Hydrogen bonding networks and proton transfer compounds of cobalt(II) and copper(II) with pyridine-2,5-dicarboxylate

Alper Tolga Çolak, Okan Zafer Yeşilel, Gönül Pamuk, Handan Günay, and Orhan Büyükgüngör

Polyhedron, 2011, Volume 30, Number 6, Page 1012

DOI: 10.1016/j.poly.2010.12.048

[6]

From Metalloligand to Extended 3D Network: Synthesis, Crystal Structure and Magnetic Property of {[Cu(en)2][Cu(μ3-pydc)2]·6H2O} n

Fatih Semerci, Okan Zafer Yeşilel, Ertan Şahin, Yusuf Yerli, and Ramazan Topkaya

Journal of Inorganic and Organometallic Polymers and Materials, 2011, Volume 21, Number 2, Page 261

DOI: 10.1007/s10904-010-9452-8

[7]

Cu(II) and Zn(II)-Pyridine-2,3-Dicarboxylate Complexes with 2-Methylimidazole: Syntheses, Crystal Structures, Spectroscopic and Thermal Analyses

Fatih Semerci, Okan Zafer Yeşilel, and Ertan Şahin

Journal of Inorganic and Organometallic Polymers and Materials, 2010, Volume 20, Number 2, Page 334

DOI: 10.1007/s10904-010-9353-x

Comments (0)

Please log in or register to comment.

General note: By using the comment function on degruyter.com you agree to our Privacy Statement. A respectful treatment of one another is important to us. Therefore we would like to draw your attention to our House Rules.

Recently viewed (1)

My CartAdded To Cart

Zeitschrift für Kristallographie - Crystalline Materials

Most Downloaded Articles

Issues

Volume 233 (2018)

Volume 232 (2017)

Volume 231 (2016)

Volume 230 (2015)

Volume 229 (2014)

Volume 228 (2013)

Volume 227 (2012)

Volume 226 (2011)

Volume 225 (2010)

Volume 224 (2009)

Volume 223 (2008)

Volume 222 (2007)

Volume 221 (2006)

Volume 220 (2005)

Volume 219 (2004)

Volume 218 (2003)

Volume 217 (2002)

Volume 216 (2001)

Volume 215 (2000)

Volume 214 (1999)

Volume 213 (1998)

Volume 212 (1997)

Volume 211 (1996)

Volume 210 (1995)

Volume 209 (1994)

Volume 208 (1993)

Volume 207 (1993)

Volume 206 (1993)

Volume 205 (1993)

Volume 204 (1993)

Volume 203 (1993)

Volume 202 (1992)

Volume 201 (1992)

Volume 200 (1992)

Volume 199 (1992)

Volume 198 (1992)

Volume 197 (1991)

Volume 196 (1991)

Volume 195 (1991)

Volume 194 (1991)

Volume 193 (1990)

Volume 190 (1990)

Volume 192 (1990)

Volume 191 (1990)

Volume 189 (1989)

Volume 188 (1989)

Volume 187 (1989)

Volume 186 (1989)

Volume 185 (1988)

Volume 184 (1988)

Volume 183 (1988)

Volume 182 (1988)

Volume 181 (1987)

Volume 180 (1987)

Volume 179 (1987)

Volume 178 (1987)

Volume 177 (1986)

Volume 176 (1986)

Volume 175 (1986)

Volume 174 (1986)

Volume 173 (1985)

Volume 172 (1985)

Volume 171 (1985)

Volume 170 (1985)

Volume 169 (1984)

Volume 168 (1984)

Volume 167 (1984)

Volume 166 (1984)

Volume 165 (1983)

Volume 164 (1983)

Volume 163 (1983)

Volume 162 (1983)

Volume 161 (1982)

Volume 160 (1982)

Volume 159 (1982)