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Zeitschrift für Naturforschung B

A Journal of Chemical Sciences

12 Issues per year


IMPACT FACTOR 2016: 0.631

SCImago Journal Rank (SJR) 2016: 0.237
Source Normalized Impact per Paper (SNIP) 2016: 0.332

Online
ISSN
1865-7117
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Volume 20, Issue 6 (Jun 1965)

Issues

Beitrag zur Chemie des Galliums The Synthesis and some Properties of Gallium Ethoxide

R. Reinmann / A. Tanner
Published Online: 2014-06-02 | DOI: https://doi.org/10.1515/znb-1965-0606

Experimental amounts in the range of 50 g each of gallium triethoxide have been prepared by reacting gallium trichloride with freshly prepared sodium ethoxide in absolute alcohol. Chloride, always present in the raw product, can be eliminated by precipitation with silver nitrate. Gallium triethoxide crystallizes in colourless needles, melting at 144.5°C. The density of the very hygroscopic product is 1.23 g/cc. It is volatile at elevated temperature in vacuum.

By alcohol interchange, the ethoxide can easily be transformed to the isopropoxide.

About the article

Received: 1965-03-06

Published Online: 2014-06-02

Published in Print: 1965-06-01


Citation Information: Zeitschrift für Naturforschung B, ISSN (Online) 1865-7117, ISSN (Print) 0932-0776, DOI: https://doi.org/10.1515/znb-1965-0606.

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© 1946 – 2014: Verlag der Zeitschrift für Naturforschung. This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License. BY-NC-ND 3.0

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