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Zeitschrift für Naturforschung B

A Journal of Chemical Sciences

12 Issues per year


IMPACT FACTOR 2016: 0.631

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Source Normalized Impact per Paper (SNIP) 2016: 0.332

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1865-7117
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Volume 41, Issue 1 (Jan 1986)

Issues

NMR-Untersuchungen an 3,3-Difluor-2-ethyI-1,1,2-tris(diethoxyphosphoryI)-cyclopropan / NMR Investigation of 3,3-Difluoro-2-ethyl-1,1,2-tris(diethoxyphosphoryl)cyclopropane

Gernot Heckmann
  • Institut für Anorganische Chemie der Universität Stuttgart, Pfaffenwaldring 55, D-7000 Stuttgart 80
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
/ Ekkehard Fluck
  • Gmelin-Institut für Anorganische Chemie der Max-Planck-Gesellschaft, Varrentrappstraße 40/42, D-6000 Frankfurt am Main 90
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
/ Jürgen Svara
  • Institut für Anorganische Chemie der Universität Stuttgart, Pfaffenwaldring 55, D-7000 Stuttgart 80
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
Published Online: 2014-06-02 | DOI: https://doi.org/10.1515/znb-1986-0113

The 19F, 31P and 13C NMR spectra in double and triple resonance mode and the temperature dependence of the NMR parameters of the title compound are discussed in detail. The rotational behavior of the phosphoryl groups is described; two of these groups show equal barriers to rotation of 75 kJ mol-1, the third one is rotating freely at room temperature.

Keywords: 3,3-Difluoro-2-ethyl-1,1,2-tris(diethoxyphosphoryl)cyclopropane. NMR Spectra; Triple Resonance

About the article

Received: 1985-09-30

Published Online: 2014-06-02

Published in Print: 1986-01-01


Citation Information: Zeitschrift für Naturforschung B, ISSN (Online) 1865-7117, ISSN (Print) 0932-0776, DOI: https://doi.org/10.1515/znb-1986-0113.

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© 1946 – 2014: Verlag der Zeitschrift für Naturforschung. This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License. BY-NC-ND 3.0

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