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Darstellung und Kristallstruktur von Bis(triphenylphosphin)-decahydro-hypho-hexaboran [(PPh3)2B6H10]·CH2Cl2 / Synthesis and Crystal Structure of Bis(triphenylphosphine)-decahydro-hypho-hexaborane[( PPh3)2B6H10]CH2Cl2

  • T. Schaper and W. Preetz

By reaction of [B6H6]2- with (PPh3)3AgCl in dichloromethane the belt-shaped hypho-hexaborane adduct [(PPh3)2B6H10] is formed. The crystal structure of [(PPh3)2B6H10]·CH2Cl2 has been determined by single crystal X-ray diffraction analysis: orthorhombic, space group Pbnb with a = 9.804(3), b = 17.864(4), c = 21.334(2) Å, Z = 4.

Received: 1998-7-9
Published Online: 2014-6-2
Published in Print: 1998-11-1

© 1946 – 2014: Verlag der Zeitschrift für Naturforschung

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