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Zeitschrift für Naturforschung B

A Journal of Chemical Sciences

12 Issues per year

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Volume 62, Issue 2


Synthesis of 3,4,5-Trimethoxy-4’-hydroxystilbene Derivatives and Crystal Structure of Ethyl {4-[(E)-2-(3,4,5-trimethoxyphenyl)vinyl]phenoxy}acetate

Li Baolin / Guo Jian / Zhang Xiquan
  • Jiangsu Chia Tai Tianqing Pharmaceutical Co., Ltd. Nanjing 210018, China c Department of Chemistry, Northwest University, Xi’an 710069, China
  • Other articles by this author:
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/ Lai Yitian / Hu Huaiming
Published Online: 2014-06-02 | DOI: https://doi.org/10.1515/znb-2007-0216

Several new 4’-O-substituted derivatives of 3,4,5-trimethoxy-4’-hydroxystilbene were synthesized and characterized by their IR and NMR spectra. The crystal structure of ethyl {4-[(E)-2-(3,4,5-trimethoxyphenyl) vinyl]phenoxy}acetate, one of these stilbene derivatives, has been solved by singlecrystal X-ray structure analysis. The results show that all carbon and oxygen atoms in the molecule are nearly coplanar except C(16), and molecules stack to a column arrangement owing to C-H···π interactions. Pairs of these columns are linked by other molecules, and these linker molecules themselves also produce a column along the other direction. A puckered cyclic tetramer R44 (46) is formed and the tetramer propagates itself via intermolecular hydrogen bonds and C-H···π interactions. In this way, molecules are interrelated and assembled to a two-dimensional layer structure.

Keywords: 3,4,5-Trimethoxy-4’-hydroxystilbene Derivatives; Crystal Structure; Hydrogen Bond

About the article

Received: 2006-08-19

Published Online: 2014-06-02

Published in Print: 2007-02-01

Citation Information: Zeitschrift für Naturforschung B, Volume 62, Issue 2, Pages 244–248, ISSN (Online) 1865-7117, ISSN (Print) 0932-0776, DOI: https://doi.org/10.1515/znb-2007-0216.

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© 1946 – 2014: Verlag der Zeitschrift für Naturforschung. This work is licensed under the Creative Commons Attribution-NonCommercial-NoDerivatives 3.0 License. BY-NC-ND 3.0

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