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Zeitschrift für Naturforschung B

A Journal of Chemical Sciences

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1865-7117
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Volume 71, Issue 1 (Jan 2016)

Issues

Structural and IR-spectroscopic characterization of magnesium acesulfamate

Oscar E. Piro
  • Facultad de Ciencias Exactas, Departamento de Física and Instituto IFLP (CONICET-CCT-La Plata), Universidad Nacional de La Plata, 1900 La Plata, Argentina
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/ Gustavo A. Echeverría
  • Facultad de Ciencias Exactas, Departamento de Física and Instituto IFLP (CONICET-CCT-La Plata), Universidad Nacional de La Plata, 1900 La Plata, Argentina
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/ Beatriz S. Parajón-Costa
  • Facultad de Ciencias Exactas, Centro de Química Inorgánica (CEQUINOR/CONICET-CCT-La Plata, UNLP), Universidad Nacional de La Plata, C. Correo 962, 1900-La Plata, Argentina
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/ Enrique J. Baran
  • Corresponding author
  • Facultad de Ciencias Exactas, Centro de Química Inorgánica (CEQUINOR/CONICET-CCT-La Plata, UNLP), Universidad Nacional de La Plata, C. Correo 962, 1900-La Plata, Argentina
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Published Online: 2015-12-07 | DOI: https://doi.org/10.1515/znb-2015-0132

Abstract

Magnesium acesulfamate, Mg(C4H4NO4S)2·6H2O, was prepared by the reaction of acesulfamic acid and magnesium carbonate in aqueous solution, and characterized by elemental analysis. Its crystal structure was determined by single crystal X-ray diffraction methods. The substance crystallizes in the triclinic space group P1̅ with one molecule per unit cell. The FTIR spectrum of the compound was also recorded and is briefly discussed. Some comparisons with other simple acesulfamate and saccharinate salts are also made.

Keywords: crystal structure; FTIR spectra; magnesium acesulfamate; synthesis

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About the article

Corresponding author: Enrique J. Baran, Facultad de Ciencias Exactas, Centro de Química Inorgánica (CEQUINOR/CONICET-CCT-La Plata, UNLP), Universidad Nacional de La Plata, C. Correo 962, 1900-La Plata, Argentina, Fax: +54-221-4259485, E-mail:


Received: 2015-08-10

Accepted: 2015-09-10

Published Online: 2015-12-07

Published in Print: 2016-01-01


Citation Information: Zeitschrift für Naturforschung B, ISSN (Online) 1865-7117, ISSN (Print) 0932-0776, DOI: https://doi.org/10.1515/znb-2015-0132.

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