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Zeitschrift für Naturforschung B

A Journal of Chemical Sciences

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1865-7117
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Volume 73, Issue 5

Issues

A heterotrimetallic Ni(II)–Dy(III) bis(salamo)-based complex: synthesis, structure and fluorescent property

Qing Zhao
  • School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou, Gansu 730070, P. R. China
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
/ Ying-Qi Pan
  • School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou, Gansu 730070, P. R. China
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
/ Xiao-Yan Li
  • School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou, Gansu 730070, P. R. China
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
/ Han Zhang
  • School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou, Gansu 730070, P. R. China
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
/ Wen-Kui Dong
  • Corresponding author
  • School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou, Gansu 730070, P. R. China
  • Email
  • Other articles by this author:
  • De Gruyter OnlineGoogle Scholar
Published Online: 2018-03-19 | DOI: https://doi.org/10.1515/znb-2017-0214

Abstract

A discrete heterotrinuclear complex [{Ni2LDy(OAc)3(CH3OH)}2] · 2CH3OH · 3CH2Cl2, with a naphthalenediol-based acyclic bis(salamo) ligand H4L, has been synthesized and structurally characterized using elemental analyses, IR, UV/Vis and fluorescence spectra and single crystal X-ray diffraction. The crystal structure shows two crystallographically independent but chemically identical molecules (molecules I and II). All the Ni(II) atoms are hexa-coordinated with slightly distorted octahedral geometries. The central Dy atoms are nona-coordinated with slightly distorted tricapped trigonal prism geometries. An infinite 3D supramolecular structure is formed via intermolecular hydrogen bonding and C–H…π interactions.

Keywords: 3d-4f complex; bis(salamo) ligand; crystal structure; fluorescence property; nickel(II)–dysprosium(III)

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About the article

Received: 2017-12-20

Accepted: 2018-01-23

Published Online: 2018-03-19

Published in Print: 2018-05-24


Citation Information: Zeitschrift für Naturforschung B, Volume 73, Issue 5, Pages 281–288, ISSN (Online) 1865-7117, ISSN (Print) 0932-0776, DOI: https://doi.org/10.1515/znb-2017-0214.

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