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Zeitschrift für Physikalische Chemie

International journal of research in physical chemistry and chemical physics

Editor-in-Chief: Rademann, Klaus


IMPACT FACTOR 2017: 1.144
5-year IMPACT FACTOR: 1.144

CiteScore 2017: 1.08

SCImago Journal Rank (SJR) 2017: 0.495
Source Normalized Impact per Paper (SNIP) 2017: 0.495

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2196-7156
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Volume 221, Issue 3

Issues

Synthesis of Monodisperse PbS Nanoparticles and Their Assembly into Highly Ordered 3D Colloidal Crystals

M. Nagel / Stephen G. Hickey / A. Frömsdorf / A. Kornowski / Horst Weller
Published Online: 2009-09-25 | DOI: https://doi.org/10.1524/zpch.2007.221.3.427

We describe the synthesis of highly monodisperse PbS nanocrystals using an organometalic approach, whereby oleic acid and tri-n-octylphosphine serve as stabilizing ligands. The optical bandgap of the particles is tunable as a function of crystal-size throughout the near-infrared region from 800 to 2200 nm. The particles were characterized using X-ray diffraction, optical spectroscopy and transmission electron microscopy. Applying the three layer super saturation technique we were able to grow colloidal crystals of various shapes as shown by scanning electron microscopy. Small-angle X-ray scattering experiments indicate fcc lattice structure.

Keywords: Nanoparticles; Self-Assembly; Colloidal Crystals

About the article

Received: 2006-11-15

Accepted: 2006-12-11

Published Online: 2009-09-25

Published in Print: 2007-03-01


Citation Information: Zeitschrift für Physikalische Chemie, Volume 221, Issue 3, Pages 427–437, ISSN (Online) 2196-7156, ISSN (Print) 0942-9352, DOI: https://doi.org/10.1524/zpch.2007.221.3.427.

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