The crystal structure of synthetic KFe[SeO3]2 was determined by single crystal X-ray diffraction methods: space group Pnma (D2h16), a = 12.948(2) Å, b = 5.430(1) Å, c = 8.069(1) Å, V = 567.31 Å3, Z = 4; 1354 unique data, measured up to 2θ = 70°; R, Rw = 0.035, 0.031. The framework structure consists of KO8 polyhedra, isolated FeO6 octahedra and trigonal pyramidal SeO3 groups.
Zeitschrift für Kristallographie – Crystalline Materials offers a place for researchers to present results of their crystallographic studies. The journal includes theoretical as well as experimental research. It publishes Original Papers, Letters and Review Articles in manifold areas of crystallography.