Crystal structure of a C2-symmetric Schiff base from 1,4-diacetyl-2,3,5,6-tetramethoxybenzene and (S)-1-phenylethylamine

Karl Peters, Eva-Maria Peters, Hans Georg von Schnering, Gerhard Bringmann and Torsten Geuder

Abstract

The title compound was prepared by a TiCl4-catalyzed reaction of bisacetylated benzene and 1-phenylethylamine. It crystallizes from ethyl acetate/petroleum ether orthorhombically in the space group P21212 with a = 796.2(1), b = 1908.7(5) and c = 924.1(2) pm.

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Zeitschrift für Kristallographie – Crystalline Materials offers a place for researchers to present results of their crystallographic studies. The journal includes theoretical as well as experimental research. It publishes Original Papers, Letters and Review Articles in manifold areas of crystallography.

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